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Submicro scale NMR sample preparation for volatile chemicals.

J Chem Ecol

November 2004

Department of Entomology, NYS Agricultural Experiment Station, Cornell University Geneva, New York, USA.

A simple, inexpensive, and highly efficient NMR sample preparation technique for volatile chemicals has been devised using a micropreparative GC system. The recovery efficiency of a volatile chemical using this technique was >80% with sample sizes of 0.05 to 0.

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