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Coordinative alignment of molecules in chiral metal-organic frameworks.
Science
August 2016
Department of Chemistry, University of California, Berkeley, CA 94720, USA. Materials Sciences Division, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA. Kavli Energy NanoSciences Institute, Berkeley, CA 94720, USA. Berkeley Global Science Institute, Berkeley, CA 94720, USA. King Abdulaziz City for Science and Technology, Riyadh 11442, Saudi Arabia.
A chiral metal-organic framework, MOF-520, was used to coordinatively bind and align molecules of varying size, complexity, and functionality. The reduced motional degrees of freedom obtained with this coordinative alignment method allowed the structures of molecules to be determined by single-crystal x-ray diffraction techniques. The chirality of the MOF backbone also served as a reference in the structure solution for an unambiguous assignment of the absolute configuration of bound molecules.
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