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Synthesis and Complexation Properties of the Anions (eta(5)-C(5)Me(5))Ru(PR(2)O)(3)(2)(-) as Ligands.
Inorg Chem
August 1998
Institute of Inorganic Chemistry, RWTH-Technical University at Aachen, Prof.-Pirlet-Strasse 1, D-52074 Aachen, Germany.
Reaction of [(eta(5)-C(5)Me(5))Ru(OMe)](2) (2) with HP(O)(OR)(2) gave the novel tripod ligands H(2)(eta(5)-C(5)Me(5))Ru{PO(OR)(2)}(3) (R = Me, Et, (i)Pr, H(2)1). H(2)(eta(5)-C(5)Me(5))Ru{PO(Ph(2))}(3) was formed with HP(O)Ph(2). [(eta(5)-C(5)Me(5))RuCl(2)](2) (3) with NaP(O)(OEt)(2) similarly gave Na(2)(eta(5)-C(5)Me(5))Ru{PO(OEt)(2)}(3) (Na(2)1; Na(2)L).
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