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Rapid, iterative syntheses of unsymmetrical di- and triarylboranes from crystalline aryldifluoroboranes.

Chem Sci

December 2023

Department of Chemistry, McGill University Otto Maass Chemistry Building, 801 Rue Sherbrooke O Montreal Quebec Canada H3A 0B8

Douglas Turnbull Marc-André Légaré

A one-pot procedure to synthesise aryldifluoroboranes, ArBF, from bench-stable arylsilanes is presented. These ArBF react conveniently with aryllithium reagents to form unsymmetrical ArAr'BF and BArAr'Ar'' in high yield. Examples of all three classes of borane have been characterised crystallographically, allowing for elucidation of geometric and crystal packing trends in crystalline ArBF.

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