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The high cost and low stability of electrocatalysts are the major challenges for the commercialization of hydrogen generation in water. In this study, we demonstrated a one-pot synthesis of a monodispersed CuPt alloy with the diameter range of 20-30 nm by a hydrothermal method. Benefiting from the more available active sites and preferable d-band structure, the CuPt alloy exhibited a superior catalytic performance than pure Pt nanoparticles (Pt NPs) in the hydrogen evolution reaction (HER).

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