Electrochemical synthesis of NiCo layered double hydroxides on nickel-coated graphite for water splitting: understanding the electrochemical experimental parameters.

The electrochemical synthesis of nickel-cobalt (Ni-Co) layered double hydroxides (LDHs) on a nickel-coated graphite support for water splitting applications was investigated. Three different electrochemical approaches, namely, cyclic voltammetry (CV), chronoamperometry (CA), and chronopotentiometry (CP), were employed for evaluating the electrodeposition of Ni-Co LDHs. The graphite support was initially coated with a thin layer of Ni by applying 50 mA cm constant current density for 120 s.