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A Green Approach: Optimization of the UPLC Method Using DoE Software for Concurrent Quantification of Pioglitazone and Dapagliflozin in a SNEDDS Formulation for the Treatment of Diabetes.
ACS Omega
November 2024
Department of Pharmaceutics, College of Pharmacy, King Saud University, Riyadh 11451, Saudi Arabia.
Clinical trials revealed that pioglitazone (PGZ) and dapagliflozin (DGZ) not only maintain normal blood glucose levels but also reduce complications of diabetes mellitus. To meet the demand for simultaneous measurement of these drugs in fixed combinations, an optimized and green UPLC method is required. The present study utilized Design of Experiments (DoE) software to optimize analytical parameters for simultaneous drug analysis.
View Article and Find Full Text PDFContaminant and residue profiles in Lebanese food: a comparative analysis with global standards.
Food Addit Contam Part A Chem Anal Control Expo Risk Assess
September 2024
Laboratory for Analysis of Organic Compounds (LAOC), CNRSL, Lebanese Atomic Energy Commission (LAEC), Beirut, Lebanon.
Lebanon's agricultural sector, known for its diverse crop and livestock production, faces challenges in the international market due to the presence of chemical residues and contaminants in its food exports. Recent rejections of these exports have raised global concerns about food safety, increasingly seen as vital for public health and economic prosperity. This review focuses on examining scientific studies about the levels of various chemical residues including pesticides, and veterinary drugs and contaminants like mycotoxins, and polycyclic aromatic hydrocarbons, and heavy metals in Lebanese food products.
View Article and Find Full Text PDFCharacteristics of built food environments associated with alternative protein food choices: a systematic review.
Int J Behav Nutr Phys Act
May 2024
Faculty of Psychology CARE-BEH Center for Applied Research On Health Behavior and Health, SWPS University, 30B Ostrowskiego Street, Wroclaw, 53238, Poland.
Background: This systematic review contributes to the understanding of the characteristics of built food environments that may be associated with choices of alternative protein foods (APF). Using the built food environment typology proposed by Downs et al., we investigated various environmental structures (e.
View Article and Find Full Text PDF[Rapid determination of 13 -blockers in health foods by ultra performance liquid chromatography-quadrupole/electrostatic field orbitrap mass spectrometry].
Se Pu
November 2023
Institute of Food Safety, Chinese Academy of Inspection and Quarantine, Beijing 100176, China.
A method based on ultra performance liquid chromatography-quadrupole/electrostatic field orbitrap mass spectrometry was developed for the rapid determination of 13 -blockers in health foods. The MS fragmentation pathways of the analytes were subsequently investigated. The optimal MS conditions, extraction solvents, mobile phases, and matrix effects were evaluated in detail.
View Article and Find Full Text PDFA sensitive ultra-performance liquid chromatography-tandem mass spectrometry method for the simultaneous quantification of assay and trace-level genotoxic tosylate analogs (methyl and ethyl) in empagliflozin and its tablet dosage forms.
Biomed Chromatogr
January 2024
Department of Chemistry, School of Science, GITAM Deemed to be University, Hyderabad, Telangana, India.
This study performed the simultaneous quantification of assay and two alkyl sulfonate (tosylate) analogs of empagliflozin (EGZ), specifically methyl 4-methyl benzene sulfonate (MMBS) and ethyl 4-methyl benzene sulfonate (EMBS) in EGZ, and its finished dosage form using an accurate and sensitive ultra-performance liquid chromatography-mass spectrometry method. The separation was achieved on a Waters Acquity BEH Shield RP18 (100 × 2.1 mm, 1.
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