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Electrochemically Driven Ugi-Azide Reaction via C(sp)-H Bond Activation of Tertiary Amines.
Org Lett
January 2025
School of Chemical Engineering, Nanjing University of Science and Technology, Nanjing, Jiangsu 210094, China.
An electrochemically driven Ugi-azide reaction was established via C(sp)-H bond activation of tertiary amines to prepare α-aminomethyl tetrazoles within 2.5 h under mild conditions with remarkable tolerance of various functional groups. Besides, this electrochemical strategy not only obviated the needs of iodine, metal, and exogenous oxidant but possessed potential applicability of convenient large-scale synthesis.
View Article and Find Full Text PDFSerum cardiac and inflammatory biomarker levels following chemotherapy among female patients with breast cancer attending at Tikur Anbessa Specialized Hospital, Addis Ababa, Ethiopia.
BMC Cancer
January 2025
Department of Biomedical Sciences, College of Medicine and Health Sciences, Bahir Dar University, Bahir Dar, P.O. Box 79, Ethiopia.
Background: Chemotherapy is a well-established therapeutic approach for several malignancies, including breast cancer (BCa). However, the clinical efficacy of this drug is limited by cardiotoxicity. Assessing multiple cardiac biomarkers can help identify patients at risk of adverse outcomes from chemotherapy.
View Article and Find Full Text PDFSea urchin-like covalent organic frameworks/TiO heterostructure for enhanced photocatalytic CO conversion.
J Colloid Interface Sci
January 2025
Key Laboratory of Functional Inorganic Material Chemistry, Ministry of Education of the People's Republic of China, School of Chemistry and Materials Science, Heilongjiang University, Harbin 150080, PR China. Electronic address:
Photocatalytic reduction of CO to valuable chemicals is an effective strategy to address the environmental problems and energy crisis. Covalent organic frameworks (COFs) are emerging materials known for their excellent diverse properties, albeit limited by special synthetic methods, including high temperature (120 °C) and the necessity of inert gas atmosphere. Herein, a novel synthesis method under room temperature and air was optimized to form TpPa-COF (TP-COF) by p-phenylenediamine (Pa) and 2,4,6-triformyl phloroglucinol (Tp) through electrostatic self-assembly.
View Article and Find Full Text PDFDyadic adjustment of persons with albinism and their significant other: A Bayesian mediation model of the Actor-Partner Interdependence (APIMeM).
Soc Sci Med
January 2025
Laboratory of Psychology (LabPsy) UR 4139, University of Bordeaux, F-33000, Bordeaux, France. Electronic address:
Background: Limited standardized empirical research exists in France on the psychosocial implications of albinism, prompting an investigation into how affected persons adapt to their disabilities. Recent advancements in health psychology have led researchers to adopt a systemic approach, considering disabilities and involving close relatives in the adaptation process. The aim of this study was to explore the mediating role of dyadic coping within family dyads, where one is a person with albinism (PWA) and the other is a close relative.
View Article and Find Full Text PDFChemical upcycling of Ni from electroplating wastewater into a well-defined catalyst for electrooxidation of glycerol to formate.
Dalton Trans
January 2025
State Key Laboratory of Chemical Resource Engineering, Beijing University of Chemical Technology, Beijing, 100029, China.
Highly effective and efficient remediation of hazardous Ni waste from electroless electroplating wastewater remains a significant challenge. However, rather than regarding it as hazardous waste, Ni-electroplating wastewater can instead be considered a huge resource of Ni. Herein, we report a convenient hydrothermal strategy for upcycling Ni from nickel-electroplating wastewater into a carbon-doped Ni-P alloy (denoted as C/Ni-P) electrocatalyst for the oxidation of glycerol to formate.
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