In this work, we aimed to study the austenite grain growth behavior of an ultra-high-strength stainless steel within the temperature range of 900-1150 °C and holding time range of 0-120 min, using a metallographic microscope and metallographic image analysis software to perform a statistical analysis of grain size variation. The undissolved phases of the steel were investigated using a field emission scanning electron microscope (SEM) and transmission electron microscope (TEM). Within the temperature range of 900-950 °C, the grain growth rate of the steel was slow, while within the range of 1000-1150 °C, the grain growth rate was relatively fast. This is attributed to the precipitation of a large number of MC-type carbides during the forging and annealing processes. In the temperature range of 900-950 °C, the solid solubility of the MC phase was low and the pinning effect was significant, which hindered the growth of austenite grains. Above 950 °C, the carbides were dissolved extensively, weakening the pinning effect on the grain boundaries and accelerating the grain growth rate. A predictive mathematical model for the growth of the original austenite grains was established based on the Arrhenius equation, elucidating the effects of heating temperature, holding time, initial grain size, and number of carbides on the growth of austenite grains, providing a theoretical basis for heat treatment process design in actual production.
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March 2025
Institute for Clean Energy and Advanced Materials, School of Materials and Energy, Southwest University, Chongqing, 400715, P. R. China.
Perovskite solar cells (PSCs) are emerging photovoltaic devices renowned for their high efficiency and low cost. Efficient and stable PSCs depend on high-quality perovskite films, which are strongly influenced by the excellent nucleation and growth. The choice of solvent is critical for the crystallization behavior of perovskite films.
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March 2025
Ion Beam Centre, Department of Physics, Kurukshetra University, Kurukshetra-136119, India.
In this study, zinc telluride (ZnTe) films were grown on quartz substrates at room temperature, 300 °C, 400 °C, 500 °C, and 600 °C using RF sputtering. The thickness of the films has been found to decrease from 940 nm at room temperature to 200 nm at 600 °C with increasing substrate temperature. The structural investigation using grazing incidence angle X-ray diffraction revealed that films deposited at room temperature are amorphous; those deposited at other substrate temperatures are polycrystalline with a cubic zincblende structure and a preferred orientation along the [111] direction.
View Article and Find Full Text PDFACS Appl Nano Mater
March 2025
Department of Chemistry, University of Massachusetts Lowell, Lowell, Massachusetts 01854, United States.
We report a fast and straightforward preparation of centimeter-sized Cu(111) from polycrystalline Cu foil by the strain-free abnormal grain growth method and the subsequent growth of monolayer graphene by chemical vapor deposition (CVD). The fabrication of Cu(111) and graphene was streamlined into a straightforward process using a CVD system consisting of a tube furnace and a quartz boat. It was found that the annealing temperature and time are critical in the growth of Cu(111).
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February 2025
Faculty of Food Science and Technology, Ho Chi Minh City University of Industry and Trade, 140 Le Trong Tan Street, Tay Thanh Ward, Tan Phu District, Ho Chi Minh City 70000, Vietnam.
Rice ( L.) is a staple food globally, providing a critical food for the majority of the Asian population. However, it exposes risks during post-harvest storage, threatening substantial losses in rice quality and quantity.
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February 2025
Institute of Agricultural Biology and Biotechnology, National Research Council, Via Moruzzi 1, 56124 Pisa, Italy.
Bee pollen is produced by honeybees from the agglutination of pollen grains belonging to one or more plant species. Although it is intended to be a nutritional source for the hive, its remarkable concentration of nutrients and phytochemicals, combined with its pleasant organoleptic qualities, makes it appealing for human consumption. This study examined the phytochemical content and the antioxidant and antimicrobial activities of a polyfloral bee pollen collected in Tuscany (Italy).
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