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Rebuttal From Drs Dabbous and Mitchell.
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Department of Political Science, University of Toronto, Toronto, ON, Canada; Division of Neurosurgery, Department of Surgery, University of Toronto, Toronto, ON, Canada.
Rebuttal From Drs Adrish and Hanania.
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Rebuttal to the article Pathological crystal structures.
Acta Crystallogr C Struct Chem
July 2024
Lawrence Berkeley National Laboratory, University of California, Berkeley, CA 94720, USA.
A section in the Acta Crystallographica Section C article by Raymond & Girolami [Acta Cryst. (2023), C79, 445-455] stated that the product of the reaction of [(Cp*Rh)(μ-OH)] (Cp* is 1,2,3,4,5-pentamethylcyclopentadiene) with 1-methylthymine (1-MT) at pH 10 and 60 °C, to synthesize the anionic component [Rh(η-N-1-MT)], was not an Rh complex, but rather an Ag complex, due to the use of silver triflate (AgOTf) to remove Cl from [Cp*RhCl] to synthesize [Cp*Rh(HO)](OTf), a water-soluble crystalline complex. We will clearly show that this premise, as stated, is invalid, while the authors have simply avoided several important facts, including that Cp*OH, a reductive elimination product, at pH 10 and 60 °C, was unequivocally identified, thus leading to the Rh anionic component [Rh(η-N-1-MT)].
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