In conventional laser-based powder bed fusion of polymers (PBF-LB/P), aging of the powder due to preheating of the powder bed is a significant issue. This paper proposes a method for low-temperature PBF-LB/P using a semi-sintering process that minimizes powder aging caused by preheating. By partially semi-sintering the low-temperature powder bed, it was possible to execute the PBF-LB/P while avoiding the aging of most of the powder. Furthermore, the suppression of curling by the semi-sintered body eliminated the need to connect the base plate to the parts, which was necessary in previously reported low-temperature PBF-LB/P. Using the semi-sintering process, we successfully built cuboid and tensile test specimens in a polyamide 11 powder bed maintained below the crystallization temperature, where the powder hardly aged. The apparent densities of the built specimens were comparable to those produced using high-temperature PBF-LB/P. However, the elongation in the building direction of the built parts by the semi-sintering process should be improved. This study represents the first step toward the practical application of low-temperature PBF-LB/P using semi-sintering.
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http://dx.doi.org/10.3390/polym16233278 | DOI Listing |
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC11644373 | PMC |
Sci Rep
December 2024
Vocational School of Technical Sciences, Akdeniz University, Antalya, Turkey.
This study examined scan speed, hatch distance, and scan rotation angle parameters to determine the effects of the powder bed fusion process on the tensile strength of AlSi10Mg material. The Taguchi L9 experimental design was applied to evaluate the effects of the parameters systematically. The experimental results revealed the importance of the parameters affecting the tensile strength of the AlSi10Mg material.
View Article and Find Full Text PDFChem Pharm Bull (Tokyo)
December 2024
School of Traditional Chinese Medicines, Shenyang Pharmaceutical University.
Enteric-coated microcapsules can protect roxithromycin (ROX) from acid hydrolysis enhancing efficacy, solubility, and dissolution rate, representing a promising oral formulation for children and patients with swallowing difficulties. ROX-layered core particles were obtained with polyvinylpyrrolidone (PVP) K30 as the binder and Eudragit L30 D-55 as the coating material using the Wurster process in a fluidized bed processor. The enteric-coated microcapsules were characterized using powder X-ray diffraction, differential scanning calorimetry, and polarized optical microscopy.
View Article and Find Full Text PDFJ Mech Behav Biomed Mater
December 2024
Department of Materials Engineering, Isfahan University of Technology, Isfahan, 84156-83111, Iran.
Zinc is a promising material for biodegradable scaffolds due to its biocompatible nature and suitable degradation rate. However, its low mechanical strength limits its use in load-bearing applications. This study aims to address this challenge by optimizing the process parameters of pure zinc using laser-based powder bed fusion and designing zinc scaffolds with tailored structures.
View Article and Find Full Text PDFMaterials (Basel)
December 2024
Department of Industrial Engineering, J.B. Speed School of Engineering, University of Louisville, Louisville, KY 40292, USA.
The simulation of additive manufacturing has become a prominent research area in the past decade. Process physics simulations are employed to replicate laser powder bed fusion (L-PBF) manufacturing processes, aiming to predict potential issues through simulated data. This study focuses on calculating surface roughness by utilizing 3D surface topology extracted from simulated data, as surface roughness significantly influences part quality.
View Article and Find Full Text PDFMaterials (Basel)
December 2024
Department of Engineering Science, University West, SE-461 86 Trollhättan, Sweden.
Additive manufacturing (AM) methods like powder bed fusion-laser beam (PBF-LB) enable complex geometry production. However, understanding and predicting the microstructural properties of AM parts remain challenging due to the inherent non-homogeneity introduced during the manufacturing process. This study demonstrates a novel approach for 3D microstructure representation and virtual testing of non-homogeneous AM materials using 2d electron backscatter diffraction (EBSD) data.
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