Crack-free Stellite-6 alloy was fabricated using the laser powder bed fusion technique equipped with a heating module as the first attempt. Single tracks were printed with a build plate heated to 400 °C to identify the processing window. Based on the melt pool dimensions, two combinations (sample A: 300 W/750 mm/s and sample B: 275 W/1000 mm/s) were identified to print the cubes. The as-printed microstructure comprised FCC-Co dendrites with MC in the interdendritic region. W-rich MC particles were found in the overlapping regions between the melt pools, matching the Scheil simulations. However, gas pores were observed due to the higher nitrogen and oxygen content of the feedstock requiring hot isostatic pressing (HIP) at 1250 °C and 150 MPa for 2 h. Sample A was partially recrystallized with slightly coarsened MC, while sample B underwent complete recrystallization followed by grain growth along with higher coarsening of the MC after HIP. The varying recrystallization behavior can be attributed to the difference in residual stresses and grain aspect ratio in the as-built condition dictated by laser power and scanning speed. The microhardness after HIP was slightly higher than its wrought counterpart, indicating no severe impact of post-processing on the properties of Stellite-6 alloy.
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http://dx.doi.org/10.3390/ma17225500 | DOI Listing |
Materials (Basel)
December 2024
Department of Physics, Faculty of Science & Technology, University of the Basque Country, UPV/EHU, Apdo. 644, 48080 Bilbao, Spain.
Shape memory alloys (SMAs) are functional materials with a wide range of applications, from the aerospace sector to the biomedical field. Nowadays, there is a worldwide interest in developing SMAs through powder metallurgy like additive manufacturing (AM), which allows innovative building processes. However, producing SMAs using AM techniques is particularly challenging because of the microstructure required to obtain optimal functional properties.
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December 2024
Graduate School of Engineering, University of Hyogo, Himeji, 671-2280, Japan.
The effect of hot isostatic pressing (HIP) on the thermoelectric power factor of zinc oxide (ZnO) has been examined. ZnO is expected to be a potential n-type oxide thermoelectric material that could enhance the thermoelectric conversion efficiency. The HIP treatment is useful for densifying the material and controlling crystal defects in the material by applying high temperatures and pressures simultaneously.
View Article and Find Full Text PDFMaterials (Basel)
December 2024
School of Engineering and Technology, Jacksonville University, Jacksonville, FL 32216, USA.
A hot isostatically pressed specimen of the A357 alloy in T6 condition has been tested for fatigue performance in situ. During testing, multiple small cracks were observed during the first cycle, both in proximity to and far from the stress concentration. These cracks have competed to form a propagating crack, forming multiple crack paths initially.
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November 2024
Physical Metallurgy and Materials Design Laboratory, Department of Mechanical Engineering and Materials Science, University of Pittsburgh, Pittsburgh, PA 15261, USA.
Angew Chem Int Ed Engl
November 2024
Department of Chemistry, University of Munich (LMU), Butenandtstraße 5-13, 81377, Munich, Germany.
Nitridophosphates have emerged as promising host compounds in the field of solid-state lighting. Their industrial relevance has increased significantly, mainly due to recent advances in synthetic approaches under medium-pressure (MP) conditions, including ammonothermal synthesis and hot isostatic pressing (HIP). In this study, we report on the synthesis and characterization of the quaternary representatives CaLiPN (x=2, 2.
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