Hierarchical structures and heterogeneous materials are found in many natural and engineered systems including additive manufacturing, alternative energy, biology and polymer science. Though the structure-function relationship is important for developing more advanced materials, structural characterization over broad length scales often requires multiple complementary measurements. Neutron far-field interferometry aims to enable multi-scale characterization by combining the best of neutron imaging with small-angle neutron scattering (SANS) via dark-field imaging. The microstructure, nominally from 1 nm to 10 μm, is averaged over each volume element ~(50 μm) in the sample, resulting in a 'tomographic SANS' measurement. Unlike in small-angle scattering, there are few analytical models to fit dark-field imaging data to extract properties of the microstructure. Fortunately, the dark field and SANS are related through a single Hankel transform. In this work, we discuss the development of a Python-based library, , that makes use of existing small-angle scattering models and a numerical implementation of the Hankel transform to simulate dark-field interferometry data. We demonstrate how this software can be used to inform researchers of viable sample sets for interferometry experiments, analyze interferometry data, and simulate raw and reconstructed interferometry images for the training of more advanced segmentation models and analysis protocols.
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http://dx.doi.org/10.1107/s1600576724001201 | DOI Listing |
Micron
January 2025
Department of Materials Science and Engineering, The Iby and Aladar Fleischman Faculty of Engineering, Tel Aviv University, Tel Aviv 6997801, Israel. Electronic address:
Atomic-scale metrology in scanning transmission electron microscopy (STEM) allows to measure distances between individual atomic columns in crystals and is therefore an important aspect of their structural characterization. Furthermore, it allows to locally resolve strain in crystals and to calibrate precisely the pixel size in STEM. We present a method dedicated to the evaluation of interplanar spacing (d-spacing) based on an algorithm including curve fitting of processed high-angle annular dark-field STEM (HAADF STEM) signals.
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January 2025
Chemistry Division, Bhabha Atomic Research, Centre, Mumbai 400085, India.
Magnetic field-dependent magnetization of highly crystalline FeO magnetic nanoparticles has been carried out to understand surface canting structures at low and room temperatures. The exchange bias () values of ∼18 to 27 Oe at 300 K for three samples prepared from different precursors are observed; and a decrease in value is obtained when the samples are measured at 5 K. However, with a decrease in temperature, coercivity () increases.
View Article and Find Full Text PDFSci Adv
January 2025
Electrical and Computer Engineering Department, University of California, Los Angeles, CA 90095, USA.
Gram staining has been a frequently used staining protocol in microbiology. It is vulnerable to staining artifacts due to, e.g.
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December 2024
The United Graduate School of Agricultural Science, Gifu University, Gifu 501-1193, Japan.
Extracellular vesicles (EVs), secreted from most cells, are small lipid membranes of vesicles of 30 to 1000 nm in diameter and contain nucleic acids, proteins, and intracellular organelles originating from donor cells. EVs play pivotal roles in intercellular communication, particularly in forming niches for cancer cell metastasis. However, EVs derived from donor cells exhibit significant heterogeneity, complicating the investigation of EV subtypes using ensemble averaging methods.
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January 2025
Breast Imaging Department, Red Cross Hospital Munich, Munich, Germany.
Background: A significant proportion of false positive recalls of mammography-screened women is due to benign breast cysts and simple fibroadenomas. These lesions appear mammographically as smooth-shaped dense masses and require the recalling of women for a breast ultrasound to obtain complementary imaging information. They can be identified safely by ultrasound with no need for further assessment or treatment.
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