Aim: Evaluating the fracture resistance of dental ceramics is essential for assessing their behavior. This study aimed to validate a custom load-to-fracture test for assessing fracture strength compared to a conventional method.
Materials And Methods: Acoustic emission testing, a non-destructive (ND) lab test, was employed to evaluate the fracture toughness (FT) of brittle materials by capturing sound waves generated by crack formation in failing samples. A total of 130 samples, divided into three types (glass sheets, zirconia sheets, and monolithic zirconia crowns), were tested. The fracture loads were measured using both custom and conventional methods.
Results: The mean fracture loads for glass sheets were 650.46 N ± 110.38 (custom) compared to 691.41 N ± 155.92 (conventional). For zirconia sheets, the values were 95.25 N ± 7.78 (custom) vs 112.75 N ± 31.26 (conventional). Monolithic zirconia crowns showed mean fracture loads of 1108.99 N ± 327.89 (custom) compared to 1292.52 N ± 271.42 (conventional). Statistically significant differences were evident in all three types, indicating lower values with custom testing for all samples.
Conclusion: The custom testing demonstrated an advantage in identifying cracks at lower loads, thereby enhancing the accuracy of fracture load values. Despite its limitations, the study suggests that the custom setup could be a viable alternative to conventional fracture load testing of brittle materials. However, further testing with more materials is recommended to enhance the results' accuracy and generalizability.
Clinical Significance: The findings indicate that the custom load-to-fracture test can provide more accurate measurements of FT in dental ceramics, which is crucial for predicting their clinical performance and longevity. How to cite this article: Haddad C, Eng JG, Zoghbi AE. The Acoustic Emission Testing in the Evaluation of Fracture Toughness of Brittle Materials. J Contemp Dent Pract 2024;25(7):617-623.
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http://dx.doi.org/10.5005/jp-journals-10024-3722 | DOI Listing |
Nat Commun
January 2025
Key Laboratory of Flexible Electronics (KLOFE) & Institute of Advanced Materials (IAM), Nanjing Tech University (NanjingTech), Nanjing, China.
Fully π-conjugated polymers consisting of plane and rigid aromatic units present a fantastic optoelectronic property, a promising candidate for printed and flexible optoelectronic devices. However, obtaining high-performance conjugated polymers with an excellent intrinsically flexible and printable capacity is a great challenge due to their inherent coffee-ring effect and brittle properties. Here, we report an asymmetric substitution strategy to improve the printable and stretchable properties of deep-blue light-emitting conjugated polymers with a strong inter-aggregate capillary interaction for flexible printed polymer light-emitting diodes.
View Article and Find Full Text PDFSci Rep
January 2025
School of New Energy, Longdong University, Qingyang, 745000, China.
In this work, taking wells LD1, LD2, and LY2 in the Laifeng-Xianfeng area as the research target, through core description, intensive core sampling, experimental analysis, imaging logging and other methods, the characteristics of graptolite zone development, organic carbon content, mineral composition, shale reservoir properties and the gas-bearing properties of the Wufeng-Longmaxi Formation shale are systematically analyzed. The main factors affecting the gas-bearing capacity of the Wufeng-Longmaxi Formation shale are extensively evaluated. The results reveal the following: ① The Wufeng-Longmaxi Formation shale, which was deposited in a deep-water shelf environment, has a large thickness (50-60 m) and a stable distribution.
View Article and Find Full Text PDFACS Macro Lett
January 2025
Department of Chemical Engineering and Materials Science, University of Minnesota, Minneapolis, Minnesota 55455, United States.
Poly(lactide) (PLA) is a promising biodegradable polymer with potential applications in single-use packaging. However, its use is limited by brittleness, and its biodegradability is restricted to industrial compost conditions due in part to an elevated glass transition temperature (). We previously showed that addition of a poly(ethylene-oxide)--poly(butylene oxide) diblock copolymer (PEO-PBO) forms macrophase-separated rubbery domains in PLA that can impart significant toughness at only 5 wt %.
View Article and Find Full Text PDFACS Appl Mater Interfaces
January 2025
Institute for Frontier Materials, Deakin University, Waurn Ponds, Victoria 3216, Australia.
Materials and devices that harvest acoustic energy can enable autonomous powering of microdevices and wireless sensors. However, traditional acoustic energy harvesters rely on brittle piezoceramics, which have restricted their use in wearable electronic devices. To address these limitations, this study involves the fabrication of acoustic harvesters using electrospinning of the piezoelectric polymer PVDF-TrFE onto fabric-based electrodes.
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December 2024
Condensed Matter Theory Group, School of Studies in Physics, Jiwaji University, Gwalior, 474 011, India.
This study presents a comprehensive investigation into the intrinsic properties of RNiP (where R = Sm, Eu) filled skutterudite, employing the full-potential linearized augmented plane wave method within density functional theory (DFT) simulations using the WIEN2k framework. Structural, phonon stability, mechanical, electronic, magnetic, transport, thermal, and optical properties are thoroughly explored to provide a holistic understanding of these materials. Initially, the structural stability of SmNiP and EuNiP is rigorously evaluated through ground-state energy calculations obtained from structural optimizations, revealing a preference for a stable ferromagnetic phase over competing antiferromagnetic and non-magnetic phases.
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