Impact of Speed Sintering on Translucency, Opalescence and Microstructure of Dental Zirconia with a Combination of 5 mol% and 3 mol% Yttria-Stabilized Zirconia.

Materials (Basel)

Department of Dental Materials, Dental and Life Science Institute, School of Dentistry, Pusan National University, Yangsan-si 50612, Republic of Korea.

Published: October 2024

Optical characteristics and microstructure of multilayered zirconia with different yttria contents in each layer can be influenced differently with a layer after speed sintering. The layer-wise translucency and opalescence of dental zirconia (E.max, E.max ZirCAD prime; Cercon, Cercon ht ML) after conventional (control) and speed sintering were analyzed using a spectrophotometer (n = 5). Specimens were subjected to microstructural analyses (n = 2) using field-emission scanning electron microscopy (FE-SEM) and phase analyses (n = 1) using high-resolution X-ray diffraction (HRXRD) and Rietveld refinement. The translucency parameter (TP) and opalescence parameter (OP) were analyzed using a 3-way ANOVA, followed by Scheffé's post hoc test (α = 0.05). The average grain size was analyzed using the Welch's -test and Kruskal-Wallis test, followed by the Bonferroni-Dunn post hoc test (α = 0.05). Changes to the TP and OP after speed sintering were only observed in the dentin layers. Although the TP of E.max increased ( < 0.05), the difference was below the 50:50% perceptibility threshold (ΔE = 0.8). The OP of E.max decreased slightly, whereas that of Cercon increased slightly ( < 0.05). The microstructure and phase fraction of both zirconia barely changed. Therefore, speed sintering is considered to have a negligible clinical impact on the optical characteristics and microstructure.

Download full-text PDF

Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC11547037PMC
http://dx.doi.org/10.3390/ma17215148DOI Listing

Publication Analysis

Top Keywords

speed sintering
20
translucency opalescence
8
dental zirconia
8
optical characteristics
8
characteristics microstructure
8
post hoc
8
hoc test
8
test 005
8
increased 005
8
sintering
5

Similar Publications

Excellent Energy Storage and Charge-Discharge Performance in (PbCa)(ZrSn)O Antiferroelectric Ceramics.

ACS Appl Mater Interfaces

January 2025

State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment, Guangdong Provincial Research Center on Smart Materials and Energy Conversion Devices, Guangdong Provincial Key Laboratory of Functional Soft Condensed Matter, School of Materials and Energy, School of Electromechanical Engineering and School of Integrated Circuits, Guangdong University of Technology, Guangzhou 510006, China.

Lead-based antiferroelectric (AFE) ceramics have the advantages of high power density, fast charge and discharge speed, and the electric-field-induced AFE-FE phase transition, making them one of the potential dielectric energy storage materials. However, the energy storage density still needs to be improved. In this work, (PbCa) (ZrSn)O (PCZS, = 0.

View Article and Find Full Text PDF

Benchtop Machining of Self-Standing Alumina Doughs for Low-Number Fabrication and Prototyping.

ACS Appl Mater Interfaces

January 2025

Faculty of Engineering and Natural Sciences, Sabanci University, Istanbul 34956, Turkey.

Cold isostatic pressing, gel casting, and protein coagulation are the most common techniques to produce green bodies prior to computer numerical control (CNC)-based machining for the near-net-scale shaping of ceramics. These methods typically involve various additives and entail several steps to create a green body that is capable of withstanding machining forces. Here, utilizing a single additive, we first introduced a facile benchtop method to generate self-standing, malleable doughs of alumina in under 2 min.

View Article and Find Full Text PDF

High Speed Sintering of Polyamide 12: From Powder to Part Properties.

Polymers (Basel)

December 2024

Fraunhofer Institute for Manufacturing Engineering and Automation IPA, Universitaetsstrasse 9, 95447 Bayreuth, Germany.

High Speed Sintering (HSS) is an additive manufacturing process with great potential to produce complex, high-quality polymer parts on an industrial scale. However, little information is currently available on the characteristics of the powder materials used and the part properties that can be achieved. This is also the case for the standard material polyamide 12 (PA 12) and the first commercially available HSS machine, the VX200 HSS.

View Article and Find Full Text PDF

The manufacturing of work parts made of powder (sintered) steels is currently widespread in industry, as it provides minimal processing allowances and high dimensional accuracy, as well as the required properties and unconventional chemical composition. At the same time, their low tensile or bending strength must be considered a serious disadvantage. In order to minimize these disadvantages, a number of strengthening technologies are used, among which is the infiltration of porous base materials with metal alloys.

View Article and Find Full Text PDF

Effect of Microsize and Nanosize TiO on Porous Mullite-Alumina Ceramic Prepared by Slip Casting.

Materials (Basel)

December 2024

Institute of Materials and Surface Engineering, Faculty of Natural Science and Technology, Riga Technical University, Paula Valdena st. 3/7, LV-1048 Riga, Latvia.

Sintered porous mullite-alumina ceramics are obtained from the concentrated suspension of powdered raw materials such as kaolin, gamma and alpha AlO, and amorphous SiO, mainly by a solid-state reaction with the presence of a liquid phase. The modification of mullite ceramic is achieved by the use of micro- and nanosize TiO powders. The phase compositions were measured using an X-ray powder diffraction (XRD) Rigaku Ultima+ (Tokyo, Japan) and microstructures of the sintered specimens were analysed using scanning electron microscopy (SEM) Hitachi TM3000-TableTop (Tokyo, Japan).

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!