Optical characteristics and microstructure of multilayered zirconia with different yttria contents in each layer can be influenced differently with a layer after speed sintering. The layer-wise translucency and opalescence of dental zirconia (E.max, E.max ZirCAD prime; Cercon, Cercon ht ML) after conventional (control) and speed sintering were analyzed using a spectrophotometer (n = 5). Specimens were subjected to microstructural analyses (n = 2) using field-emission scanning electron microscopy (FE-SEM) and phase analyses (n = 1) using high-resolution X-ray diffraction (HRXRD) and Rietveld refinement. The translucency parameter (TP) and opalescence parameter (OP) were analyzed using a 3-way ANOVA, followed by Scheffé's post hoc test (α = 0.05). The average grain size was analyzed using the Welch's -test and Kruskal-Wallis test, followed by the Bonferroni-Dunn post hoc test (α = 0.05). Changes to the TP and OP after speed sintering were only observed in the dentin layers. Although the TP of E.max increased ( < 0.05), the difference was below the 50:50% perceptibility threshold (ΔE = 0.8). The OP of E.max decreased slightly, whereas that of Cercon increased slightly ( < 0.05). The microstructure and phase fraction of both zirconia barely changed. Therefore, speed sintering is considered to have a negligible clinical impact on the optical characteristics and microstructure.
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http://dx.doi.org/10.3390/ma17215148 | DOI Listing |
ACS Appl Mater Interfaces
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State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment, Guangdong Provincial Research Center on Smart Materials and Energy Conversion Devices, Guangdong Provincial Key Laboratory of Functional Soft Condensed Matter, School of Materials and Energy, School of Electromechanical Engineering and School of Integrated Circuits, Guangdong University of Technology, Guangzhou 510006, China.
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January 2025
Faculty of Engineering and Natural Sciences, Sabanci University, Istanbul 34956, Turkey.
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Fraunhofer Institute for Manufacturing Engineering and Automation IPA, Universitaetsstrasse 9, 95447 Bayreuth, Germany.
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Institute of Mechanical Engineering, University of Zielona Gora, 4 Prof. Z. Szafrana Street, 65-516 Zielona Gora, Poland.
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Institute of Materials and Surface Engineering, Faculty of Natural Science and Technology, Riga Technical University, Paula Valdena st. 3/7, LV-1048 Riga, Latvia.
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