The structure and electron emission properties of scanning tunneling microscope tips electrochemically etched from polycrystalline and recrystallized tungsten wires were investigated using scanning electron microscopy and transmission electron microscopy. Tips etched using the recrystallized wire had single crystal domains larger than those seen in tips etched from the cold drawn wire. The stability of the tips under high electric fields was investigated using field emission. It was found that tips etched from the recrystallized wire tended to have improved stability compared to those etched from the polycrystalline wire and that annealing either type of tip to high temperature in ultra-high vacuum had the greater influence on tip stability.
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http://dx.doi.org/10.1063/5.0196497 | DOI Listing |
ACS Omega
November 2024
Advanced Laboratory of Electro-Optics (ALEO), Department of Applied Physics/Electro-Optics Engineering, Lev Academic Center, Jerusalem 9116001, Israel.
Plasmonic nanostructure arrays, designed for performance as pixels in an advanced SERS imaging device, were fabricated by gallium focused ion beam (FIB). Though the FIB is best suited for etching holes and negative structures, our previously reported simulations favor protrusions. Herein, we report on the FIB methodology to "sculpt" positive structures by "ion-blasting" away the surrounding material.
View Article and Find Full Text PDFRev Sci Instrum
October 2024
Department of Mathematical and Physical Sciences, School of Computing, Engineering and Mathematical Sciences, La Trobe University, Bundoora 3086, VIC, Australia.
The structure and electron emission properties of scanning tunneling microscope tips electrochemically etched from polycrystalline and recrystallized tungsten wires were investigated using scanning electron microscopy and transmission electron microscopy. Tips etched using the recrystallized wire had single crystal domains larger than those seen in tips etched from the cold drawn wire. The stability of the tips under high electric fields was investigated using field emission.
View Article and Find Full Text PDFJ Hazard Mater
October 2024
MARA Key Laboratory for Quality and Safety Control of Poultry Products, Institute for Quality & Safety and Standards of Agricultural Products Research, Jiangxi Academy of Agricultural Sciences, Nanchang, Jiangxi 330200, China. Electronic address:
Talanta
December 2024
State Key Laboratory of Electroanalytical Chemistry, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, Changchun, 130022, PR China; University of Science and Technology of China, Hefei, 230026, PR China. Electronic address:
Accurate assessment of Total Antioxidant Capacity (TAC) in food is crucial for evaluating nutritional quality and potential health benefits. This study aims to enhance the sensitivity and reliability of TAC detection through a dual-signal method, combining colorimetric and photothermal signals. Gold nanorods (AuNRs) were utilized to establish a dual-signal method duo to the colorimetric and photothermal properties.
View Article and Find Full Text PDFJ Neural Eng
August 2024
Department of Electrical and Computer Engineering, University of Utah, Salt Lake City, UT, United States of America.
Optogenetics allows the manipulation of neural circuitswith high spatial and temporal precision. However, combining this precision with control over a significant portion of the brain is technologically challenging (especially in larger animal models).Here, we have developed, optimised, and tested, the Utah Optrode Array (UOA), an electrically addressable array of optical needles and interstitial sites illuminated by 181LEDs and used to optogenetically stimulate the brain.
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