"MightyLev," a new multi-emitter ultrasonic acoustic levitation device capable of extremely stable levitation of materials of density up to at least 11.3 g cm-3, is described. The exceptional stability of medium- to high-density samples levitated in MightyLev makes the device highly suitable for chemical and structural analysis using micro-focused spectroscopic and x-ray scattering techniques. In combination with mid-infrared laser heating, MightyLev is capable of levitating metallic and oxide materials during high-temperature cycling and melting above 1500 K. Instabilities in particle confinement during heating were investigated by directly visualizing the acoustic field using schlieren imaging. The results reveal jets of hot-air directed along the anti-nodes of the acoustic field. The reaction force on the sample from the jet, coupled with the restoring force of the acoustic trap, generates a parametric lateral oscillation of the sample. This result provides valuable insight for future optimization and wider application of acoustic levitation for high-temperature containerless material processing.
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http://dx.doi.org/10.1063/5.0221899 | DOI Listing |
Rev Sci Instrum
November 2024
Department of Physics and Astronomy, Louisiana State University, Baton Rouge, Louisiana 70803, USA.
As new alloys are being developed for additive manufacturing (AM) applications, questions related to the temperature-dependent structural and compositional stability of these alloys remain. In this work, the benefits and limitations of a unique method for testing this stability are presented. This system employs the use of polychromatic synchrotron light to perform energy-dispersive x-ray diffraction (ED-XRD) on an electrostatically levitated sample at high temperatures.
View Article and Find Full Text PDFPhys Rev E
September 2024
School of Physical Science and Technology, Northwestern Polytechnical University, Xi'an 710072, China.
The liquid state thermophysical properties and amorphous solidification kinetics of Fe_{50-x}Co_{x}Cr_{14}Mo_{14}C_{9}B_{8}Tm_{5} (x=10, 15, 20, and 25) alloys were explored by electromagnetic and electrostatic levitation techniques. It was found that the surface tension of liquid alloys with Fe contents below 30 at. % had a strong temperature dependence.
View Article and Find Full Text PDFRev Sci Instrum
October 2024
School of Physics, University of Bristol, H H Wills Physics Laboratory, Tyndall Avenue, Bristol BS8 1TL, United Kingdom.
NPJ Microgravity
May 2023
Institute of Functional Nanosystems, Ulm University, Ulm, Germany.
Transitions from the liquid to the solid state of matter are omnipresent. They form a crucial step in the industrial solidification of metallic alloy melts and are greatly influenced by the thermophysical properties of the melt. Knowledge of the thermophysical properties of liquid metallic alloys is necessary in order to gain a tight control over the solidification pathway, and over the obtained material structure of the solid.
View Article and Find Full Text PDFSci Rep
March 2022
Division of Biology and Chemistry, Paul Scherrer Institut, 5232, Villigen-PSI, Switzerland.
Acoustic levitation has attracted attention in terms of chemical and biochemical analysis in combination with various analytical methods because of its unique container-less environment for samples that is not reliant on specific material characteristics. However, loading samples with very high viscosity is difficult. To expand the scope, we propose the use of polymer thin films as sample holders, whereby the sample is dispensed on a film that is subsequently loaded onto an acoustic levitator.
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