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Protocol for hydroxylating aryl chlorides catalyzed by photouranium with water under ambient conditions. | LitMetric
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Protocol for hydroxylating aryl chlorides catalyzed by photouranium with water under ambient conditions.

Chengliang Li Leiyang Bai Xuefeng Jiang

STAR Protoc

Hainan Institute of East China Normal University, State Key Laboratory of Petroleum Molecular & Process Engineering, Shanghai Key Laboratory of Green Chemistry and Chemical Process, School of Chemistry and Molecular Engineering, East China Normal University, 3663 North Zhongshan Road, Shanghai 200062, P.R. China; School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P.R. China; State Key Laboratory of Organometallic Chemistry, Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences, 345 Lingling Road, Shanghai 200032, P.R. China. Electronic address:

Published: September 2024

Here, we present a protocol for the hydroxylation of aryl chlorides catalyzed by photouranium with water under ambient conditions. We describe steps for gram-scale hydroxylation of 2'-chloroacetophenone using our self-designed continuous-flow photoreactor. We then detail procedures for obtaining 2'-hydroxyacetophenone using our self-designed rapid separation and purification instrument. This protocol is not suitable for polycyclic and heterocyclic aryl chlorides. For complete details on the use and execution of this protocol, please refer to Sun et al..

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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC11467657PMC
http://dx.doi.org/10.1016/j.xpro.2024.103279DOI Listing

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