The exploration of short-wave ultraviolet (SUV; λ < 280 nm) transparent phosphates with substantial birefringence is crucial for the advancement of SUV laser industry. Despite their SUV transparency and potential for constructing materials with large birefringence, open-framework (OF) phosphates have rarely been explored for their birefringent properties. Herein, through a systematic exploration in this field, a new ethylenediamine-based OF zincophosphate, Na(CHN)[Zn(PO)(HPO)] (NEZPO), has been developed. NEZPO exhibits remarkable SUV transparency and significant birefringence (Δ = 0.060 at 546 nm), highlighting the potential for the development of benign SUV crystals within the OF phosphates family.
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