Metallic elemental analyses are needed to complete food composition databases, in which humans consume food to obtain energy and be able to do everyday work. The study aimed to investigate the concentrations of some metals (K, Al, Fe, Cu, Cd, and Pb) in teff and barley samples using flame atomic absorption spectroscopy (FAAS) techniques. The samples, weighing 0.5 grams each, were subjected to wet digestions using a mixture ratio of 7:3(vol/vol) of HNO to HO reagents at 90°c for 3:00 h under optimal conditions. The reagents were used to digest food samples for the presence of specific metallic elements. Flame Atomic Absorption Spectroscopy (FAAS) was used to analyze the mineral contents of the digested samples. The results demonstrated that the relative concentrations obtained in these cereal crops are different from one another. The concentration of metallic elements in mg/kg of K (2709.6±3.3), Al (952.3±4.2), Fe (320.9±4.8), Cu (25.3±3.2), Pb (ND) and Cd (ND) for red teff, K (3053.7±1.6), Al (1095.2±4.2), Fe (271.6±4.8), Cu (60.1±3.2), Pb (ND) and Cd (ND) for white teff while K (4333.3±3.2), Al (2595.2±4.2), Fe (74.0±0.00), Cu (10.5±1.8), Pb (ND) and Cd (ND) for barley. The high content of potassium and aluminum metallic elements was found in barley cereals. The results of this study will be useful in enriching the database of Ethiopian cereals as foods, advancing the knowledge of cereals and deepening the scientific understanding of the cereals.
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http://dx.doi.org/10.1016/j.apradiso.2024.111401 | DOI Listing |
Environ Monit Assess
December 2024
Chemistry Department, Faculty of Art and Science, Yıldız Technical University, 34220, Istanbul, Türkiye.
In this study, a preconcentration strategy based on Ni(OH) nanoflowers (NFs) was developed for the extraction/separation of bismuth ions from environmental water samples before the determination by flame atomic absorption spectrometry (FAAS). The homogeneous coprecipitation method was employed for the synthesis of the flower-shaped Ni(OH) and used as an adsorbent for the preconcentration of bismuth. The extraction variables were determined by a univariate optimization strategy to obtain maximum extraction performance.
View Article and Find Full Text PDFOpen Vet J
November 2024
Department of Pathology and Poultry Disease, College of Veterinary Medicine, University of Diyala, Baqubah, Iraq.
Polymers (Basel)
December 2024
Institute of Atomic Energy NNC RK, Kurchatov 140000, Kazakhstan.
This work presents the results of a study on the influence of fillers on the neutron absorption capacity of materials made from ultra-high molecular weight polyethylene (UHMWPE). Composite materials based on UHMWPE were obtained using gas-flame technology with the addition of powdered UHMWPE fillers (HBO, WC, and PbO). A radiation cassette has been developed and constructed for conducting studies on the neutron absorption capacity of the material, allowing for the placement of a sample with activation indicators.
View Article and Find Full Text PDFJ Colloid Interface Sci
December 2024
Key Laboratory for Ultrafine Materials of Ministry of Education, Shanghai Environmental, Friendly Materials Technical Service Platform, School of Materials Science and Engineering, East China University of Science and Technology, Shanghai 200237, China.
Single-atom catalysts (SACs) have garnered considerable interest in the field of heterogeneous catalysis. This study detail the synthesis of single-atom Pd catalysts supported on metal oxides using the Flame Spray Pyrolysis (FSP) method. This technique allows for the preparation of TiO with abundant oxygen vacancies by incorporating a hydrogen-rich atmosphere at high temperature (>2000 K) utilizing the quenching ring, which enhances the catalyst synthesis process.
View Article and Find Full Text PDFMicrosc Res Tech
December 2024
Department of Environmental Sciences, Shaheed Benazir Bhutto University, Dir Upper, Khyber Pakhtunkhwa, Pakistan.
This paper reports on batch investigations utilizing activated carbon (AC) made from waste Styrofoam to adsorb aluminum (Al) from aqueous solutions. The AC morphology and structure were examined using Fourier-transform infrared spectroscopy, scanning electron microscopy, and surface area analysis. The factors affecting the performance of adsorption were thoroughly examined.
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