Microwave impedance microscopy (MIM) is an emerging scanning probe technique for nanoscale complex permittivity mapping and has made significant impacts in diverse fields. To date, the most significant hurdles that limit its widespread use are the requirements of specialized microwave probes and high-precision cancellation circuits. Here, we show that forgoing both elements not only is feasible but also enhances performance. Using monolithic silicon cantilever probes and a cancellation-free architecture, we demonstrate Johnson-noise-limited, drift-free MIM operation with 15 nm spatial resolution, minimal topography crosstalk, and an unprecedented sensitivity of 0.26 zF/√Hz. We accomplish this by taking advantage of the high mechanical resonant frequency and spatial resolution of silicon probes, the inherent common-mode phase noise rejection of self-referenced homodyne detection, and the exceptional stability of the streamlined architecture. Our approach makes MIM drastically more accessible and paves the way for advanced operation modes as well as integration with complementary techniques.
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http://dx.doi.org/10.1038/s41467-024-49405-8 | DOI Listing |
Sci Rep
January 2025
Microwave Engineering Department, Electronics Research Institute (ERI) Cairo, Cairo, Egypt.
This paper presents a novel design approach for an anomalous reflector metasurface for communication systems operating at 8 GHz band. The main contribution of this work is the development of a general analytical method that accurately calculates the electromagnetic response of realistic metasurfaces with periodic impedance profiles. The modulated surface impedance is achieved by incorporating appropriately sized conductive patches on a grounded dielectric substrate.
View Article and Find Full Text PDFACS Appl Mater Interfaces
January 2025
Key Laboratory of Advanced Metallic Materials of Jiangsu Province, School of Materials Science and Engineering, Southeast University, Nanjing 211189, P. R. China.
Gradient structures are effective for microwave absorbing but suffer from inadequate lightweight and poor flexibility, making them fall behind the comprehensive requirements of electromagnetic protection. Herein, we propose a hierarchical gradient structure by integration with porous and sandwich structures. Specifically, polyimide (PI) foams are used as a robust and flexible skeleton, in which the foam cell walls are sandwiched by TiCT, ZnO, and ZrO atomic layers in sequence.
View Article and Find Full Text PDFSmall
December 2024
Shaanxi Key Laboratory of Macromolecular Science and Technology, School of Chemistry and Chemical Engineering, Northwestern Polytechnical University, Xi'an, 710072, P. R. China.
The demand for temperature-robust electromagnetic wave (EMW) absorption materials is escalating due to the varying operational temperatures of electronic devices, which can easily soar up to 100 °C, significantly affecting EMW interference management. Traditional absorbers face performance degradation across broad temperature ranges due to alterations in electronic mobility and material impedance. This study presented a novel approach by integrating semiconductor metal-organic frameworks (SC-MOFs) with paraffin wax (PW), leveraging the precise control of interlayer spacing in SC-MOFs for electron mobility regulation and the introduction of paraffin wax for temperature-inert electromagnetic properties.
View Article and Find Full Text PDFSci Rep
December 2024
Department of Electrical Engineering, Chalmers University of Technology, Gothenburg, Sweden.
This study presents the design of a high-gain 16 × 16-slot antenna array with a low sidelobe level (SLL) using a tapered ridge gap waveguide feeding network for Ka-band applications. The proposed antenna element includes four cavity-backed slot antennas. A tapered feeding network is designed and utilized for unequal feeding of the radiating elements.
View Article and Find Full Text PDFJ Colloid Interface Sci
December 2024
Department of Chemistry, Fu Jen Catholic University, New Taipei City 24205, Taiwan.
A novel metal-organic framework (MOF), (Cu-S)MOF, with a copper-sulfur planar structure was applied to photocatalytic H production application. (Cu-S)MOF@ZnS nanocomposite was synthesized using a microwave-assisted hydrothermal approach. The formation of (Cu-S)MOF and wurtzite ZnS in the composite nanoparticles was analyzed by X-ray diffraction (XRD), field emission-scanning electron microscopy (FESEM), and high-resolution transmission electron microscope (HRTEM).
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