The first total synthesis and absolute configuration assignment of asperilactone B (I) have been accomplished. Additionally, a revision of the absolute stereochemistry of asperilactone C has been done. The first total synthesis of the opposite enantiomer of asperilactone B (-I) has also been achieved, as well as that of C-7 epimers of both asperilactones B (8) and C (9).
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| http://dx.doi.org/10.1039/d4ob00583j | DOI Listing |
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