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| http://dx.doi.org/10.1002/ansa.202200901 | DOI Listing |
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Comprehensive characterization of phytochemicals and biological activities of the Italian ancient apple 'Mela Rosa dei Monti Sibillini'.
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School of Pharmacy, University of Camerino, Via S. Agostino 1, 62032 Camerino, Italy.
This study was carried out to characterize extracts from nine samples of the apple 'Mela Rosa dei Monti Sibillini' (MR) and to assess the antioxidant and anti-inflammatory activities. The extracts were analysed by High Performance Liquid Chromatography coupled with photodiode array detector and mass spectrometry (HPLC-DAD-MS) for 20 phytochemicals. The extracts from the lyophilized material (ELM) were richer in polyphenolic compounds than the dried ones (EDM).
View Article and Find Full Text PDFSame analytical method for both (bio)assay and zone isolation to identify/quantify bioactive compounds by quantitative nuclear magnetic resonance spectroscopy.
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Chair of Food Science Institute of Nutritional Science and Interdisciplinary Research Center, Justus Liebig University Giessen, Heinrich-Buff-Ring 26-32, 35392, Giessen, Germany; TransMIT Center of Effect-Directed Analysis, Kerkrader Straße 3, 35394, Giessen, Germany. Electronic address:
Differing sensitivity is the main obstacle for a direct combination of HPTLC with NMR spectroscopy. A sufficient amount of the isolated compound zone must be provided by HPTLC for subsequent offline NMR detection (HPTLC//NMR). To fill the gap, a straightforward procedure was developed using the same analytical HPTLC system for both bioprofiling and isolation of bioactive zones from multicomponent mixtures.
View Article and Find Full Text PDFSorbent-excluding sample preparation method for GC-MS pesticide analysis in apple peel.
Biomed Chromatogr
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Department of Agricultural and Environmental Sciences-Production, Landscape, Agroenergy -University of Milano, Milan, Italy.
Apple peel is frequently exposed to pesticides, especially in the last stages of the pesticide treatment practice. For a certain period, peel retains most of the applied pesticides, which precisely indicates the presence of pesticide residues. This study was conducted to establish and evaluate the method for the residue analysis of pyrimethanil, cyprodinil, trifloxystrobin, bifenthrin and boscalid by GC-MS in peel of Granny Smith, Golden Delicious and Idared varieties.
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