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| http://dx.doi.org/10.1007/s40863-022-00307-x | DOI Listing |
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Diversified Fluoroalkylation of Alkenes Using Quaternary Fluoroalkyl Alcohols as the Fluoroalkylating Reagents.
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Shanghai Frontiers Science Center of Drug Target Identification and Delivery, School of Pharmaceutical Sciences, Shanghai Jiao Tong University, Shanghai, 200240, China.
Given the widespread presence of fluoroalkyl functionalities in bioactive molecules, the development of fluoroalkylation reactions with bench-stable and easy-to-use fluoroalkylating reagents is highly desirable. In addition, realization of mono-, di-, tri-, or polyfluoroalkyation usually requires distinct types of fluoroalkylating reagents under different or even harsh reaction conditions, and a universal method to accomplish different hydrofluoroalkylation of alkenes is lacking. Herein, the use of quaternary fluoroalkyl alcohols is reported as the universal fluoroalkylating reagents to readily facilitate mono-, di-, tri-, or polyfluoroalkylation of a wide range of alkene substrates in high yields.
View Article and Find Full Text PDFPlatelet rich fibrin three-layer reconstruction of the sellar floor after endoscopic endonasal transsphenoidal approach: technical note and initial experience.
Front Surg
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Department of Neurosurgery, Faculty of Medicine, Medical Center, University of Freiburg, Freiburg, Germany.
Background: Cerebrospinal fluid (CSF) leakage frequently complicates endoscopic endonasal transsphenoidal pituitary resections, despite the use of lumbar drains, nasoseptal flaps, or commercial dura sealants. Managing this complication often requires revision surgery and increases the risk of infection. Platelet-rich fibrin (PRF), an affordable autologous biomaterial derived from the patient's blood through short, angulated centrifugation, contains growth factors and leukocytes embedded in a fibrin matrix.
View Article and Find Full Text PDFIntra-aural swallowing sound analysis with simultaneous videofluoroscopy and cervical swallowing sound recording.
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Department of Otolaryngology/Head and Neck Surgery, Kyushu University Hospital, 3-1-1, Maidashi, Higashi-ku, Fukuoka 812-8582, Japan.
Objective: Haji et al. reported that characteristic click-like sounds during the swallowing reflex were recorded with a small lavalier microphone placed in the ear. They also reported that endoscopic and phototubometric observations showed that these sounds were likely related to the opening and closing of the Eustachian tube during swallowing.
View Article and Find Full Text PDFTranscostal Microendoscopic Discectomy for Central Thoracic Disc Herniation Causing Myelopathy: A Technical Note.
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Department of Orthopaedic Surgery, Wakayama Medical University, Wakayama, Japan.
Introduction: Minimally invasive surgical treatment of myelopathy caused by central thoracic disc herniation (TDH) is challenging to carry out because reaching the herniation site is difficult and the thoracic spinal cord is fragile. In this study, using the posterior-lateral approach for central TDH with myelopathy, we present a novel procedure of transcostal microendoscopic discectomy (TCMED).
Technical Note: The patient was operated in a prone position under general anesthesia.
Effect of hay nets on subluxations, pain-pressure thresholds, and cervical range of motion in the axial skeleton of adult horses.
J Equine Vet Sci
December 2024
University of Minnesota - Twin Cities, Department of Animal Science, 1364 Eckles Avenue, St. Paul, MN 55108, United States.
Article Synopsis
- Horses were studied to see how using hay nets affects their health, specifically looking at skeletal issues and pain thresholds.
- In a year-long study, 13 horses were divided into two groups, one with hay nets and the other without, and changes in their health metrics were evaluated.
- Results showed that while horses with hay nets had slightly more cervical subluxations, they also exhibited better cervical range of motion, indicating that using hay nets may have minimal impacts on horse health overall.
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