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Transformation of Mononuclear Plutonium(III) Tetrazolate Complexes into Dinuclear Complexes in the Solid State. | LitMetric
The salt metathesis reaction of Na(pmtz)·HO [pmtz 5-(pyrimidyl)tetrazolate] and PuBr·HO in an aqueous media leads to the formation of the mononuclear compound [Pu(pmtz)(HO)]·(3 + ) HO (, = ∼8) that is isotypic with the lanthanide compounds [Ln(pmtz)(HO)]·(3 + ) HO (Ln = Ce-Nd). Dissolution and recrystallization of in water yields the dinuclear compound {[Pu(pmtz)(HO)](μ-pmtz)}(pmtz)·14HO (), which is isotypic with the lanthanide compounds {[Ln(pmtz)(HO)](μ-pmtz)}(pmtz)·14HO (Ln = Nd and Sm). Like their nine-coordinate ionic radii, the M-O and M-N bond lengths in / and /, respectively, are within error of one another. The Laporte-forbidden 4f → 4f and 5f → 5f transitions are also assigned in the UV-vis-NIR spectra for these -element tetrazolate coordination compounds.
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