In this study, [DABCO](SOH)CuCl as a novel DABCO-based molten salt with dual acidic functionality (Brønsted and Lewis) has been synthesized, characterized and used as a high-performance catalyst in the one-pot synthesis of 3,4-dihydropyrimidine and polyhydroquinoline derivatives. The identification of this catalyst was accomplished by using techniques such as infrared spectroscopy (FT-IR), X-ray diffraction (XRD), thermo gravimetric analysis (TGA), field emission scanning electron microscopy (FESEM) and energy dispersive X-ray (EDS) spectroscopy. Excellent efficiency, short reaction times, a simple working method and also use of a recyclable catalyst are the considerable advantages of this process.
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http://www.ncbi.nlm.nih.gov/pmc/articles/PMC10699162 | PMC |
http://dx.doi.org/10.1039/d3ra07366a | DOI Listing |
RSC Adv
November 2023
Department of Chemistry, College of Sciences, University of Guilan Rasht 41335-19141 Iran +98 131 3233262 +981313233262.
In this study, [DABCO](SOH)CuCl as a novel DABCO-based molten salt with dual acidic functionality (Brønsted and Lewis) has been synthesized, characterized and used as a high-performance catalyst in the one-pot synthesis of 3,4-dihydropyrimidine and polyhydroquinoline derivatives. The identification of this catalyst was accomplished by using techniques such as infrared spectroscopy (FT-IR), X-ray diffraction (XRD), thermo gravimetric analysis (TGA), field emission scanning electron microscopy (FESEM) and energy dispersive X-ray (EDS) spectroscopy. Excellent efficiency, short reaction times, a simple working method and also use of a recyclable catalyst are the considerable advantages of this process.
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