Purpose: This study aimed to assess and compare the color stability, flexural strength (FS), and surface roughness of occlusal splints fabricated from heat-cured acrylic resin, milled polymethyl methacrylate (PMMA)-based resin, and 3D-printed (PMMA) based-resin.
Materials And Methods: Samples of each type of resin were obtained, and baseline measurements of color and surface roughness were recorded. The specimens were divided into three groups (n = 10) and subjected to distinct aging protocols: thermomechanical cycling (TMC), simulated brushing (SB), and control (without aging). Final assessments of color and surface roughness and three-point bending test (ODM100; Odeme) were conducted, and data were statistically analyzed (2-way ANOVA, Tukey, <.05).
Results: Across all resin types, the most significant increase in surface roughness (Ra) was observed after TMC ( < .05), with the 3D-printed resin exhibiting the lowest Ra ( < .05). After brushing, milled resin displayed the highest Ra ( < .05) and greater color alteration (ΔE) compared to 3D-printed resin. The most substantial ΔE was recorded after brushing for all resins, except for heat-cured resin subjected to TMC. Regardless of aging, milled resin exhibited the highest FS ( < .05), except when compared to 3D-printed resin subjected to TMC. Heat-cured resin exposed to TMC demonstrated the lowest FS, different ( < .05) from the control. Under control conditions, milled resin exhibited the highest FS, different ( < .05) from the brushed group. 3D-printed resin subjected to TMC displayed the highest FS ( < .05).
Conclusion: Among the tested resins, 3D-printed resin demonstrated superior longevity, characterized by minimal surface roughness and color alterations. Aging had a negligible impact on its mechanical properties.
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http://dx.doi.org/10.4047/jap.2023.15.5.227 | DOI Listing |
ACS Appl Mater Interfaces
January 2025
School of Engineering, RMIT University, Bundoora, VIC 3083, Australia.
Graphene and its derivatives have been widely used as reinforcing nanofillers for high-performance polymer nanocomposites. The effectiveness of the reinforcement largely depends on the properties of the nanofiller-matrix interface, which can be represented by the interfacial shear strength (IFSS). This work systematically investigates IFSS enhancements for polyethylene (PE) nanocomposites reinforced by graphene origami (GOri) through molecular dynamics pull-out simulations.
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January 2025
Centre for Opto/Bio-Nano Measurement and Manufacturing, Zhongshan Institute of Changchun University of Science and Technology, Zhongshan, China.
When protein molecules come into contact with different types of substrate materials, the surface properties of the substrate will have a significant effect on their self-assembly behavior. The purpose of this study was to investigate the self-assembly behavior of zein molecules on the two different substrates. Herein, the microstructure of zein molecules on the surface of two typical substrates, mica and glass, were characterized in detail by atomic force microscopy.
View Article and Find Full Text PDFLangmuir
January 2025
Natural Environment Experimental Research Center in Turpan, Xinjiang Uygur Autonomous Region, Turpan 838000, China.
In this study, the degradation behavior of poly(lactic acid) nanocomposite films (PLA/Hec-g@PS) under extreme natural environments was investigated, and the degraded PLA based films were applied to adsorb Cu(II). During the early and midstages of degradation, the surface roughness and crack propagation rate of PLA/Hec-g@PS films were significantly lower than those of PLA films. This could be due to the fact that Hec-g@PS enhanced the interaction forces between C-O-C + CH and C═O in the PLA chains, thereby mitigating the degradation of PLA.
View Article and Find Full Text PDFTalanta
December 2024
Wuhan National Laboratory for Optoelectronics (WNLO), Huazhong University of Science and Technology, Wuhan, 430074, PR China. Electronic address:
Magnesium plays an important role in the hardening mechanism of aluminum alloys, but sensitisation-induced intergranular corrosion cracking limits the widespread use of aluminum alloy in equipment. For on-site quantitative assessment of sensitisation in 5-series aluminum alloys, a laser-induced plasma imaging technique is proposed, which evaluates the degree of aluminum alloy sensitisation by obtaining images of the plasma formed by laser ablation of aluminum alloys, and then classifying and quantifying the images using a residual network. Compared to EMAT, XRD, ECT and LIBS techniques, the sample surface only needs to be polished, does not consume chemical reagents and is not affected by the shape and thickness of the workpiece, which provides higher quantitative accuracy, stability and detection efficiency.
View Article and Find Full Text PDF3D Print Addit Manuf
October 2024
State Key Laboratory of Materials Processing and Die and Mould Technology, School of Materials Science and Engineering, Huazhong University of Science and Technology, Wuhan, China.
The optimization of slurry content and forming process parameters has a significant effect in slurry microextrusion direct forming method. In this article, magnesium sulfate monohydrate (MgSO) and polyvinylpyrrolidone (PVP) were used as raw materials to prepare the slurry, and the component ratios of the slurry and the optimization of its forming process were discussed. The optimum slurry content is 64 wt.
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