Cross-validation of standardisation techniques at ANSTO using cobalt-60 and learnings from the presence and identification of non-gamma-ray emitting impurities.

Appl Radiat Isot

Australian Nuclear Science and Technology Organisation, New Illawarra Rd, Lucas Heights, 2234 NSW, Australia.

Published: November 2023

To fulfil the technical requirements for accreditation to ISO/IEC 17025, the end-to-end validation of all processes associated with standardising Co, including gravimetric source dispensing, primary standardisation by the 4π(LS)β-γ coincidence and live-timed anti-coincidence extrapolation techniques, and impurity determination were performed and documented. Pure-beta-emitting impurities in a Co stock solution were identified. The impact of such impurities on measurement by liquid scintillation counting and comparison in the ESIR are discussed. A fresh Co source was produced, standardised, and compared using the SIR.

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http://dx.doi.org/10.1016/j.apradiso.2023.111027DOI Listing

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