Carbon nanotubes (CNTs) can be incorporated in various materials to enhance their mechanical or electrical properties. Information on their precise concentration and local distribution is difficult to access non-invasively. For example, electron microscopy studies require cutting of samples. Another way to measure the concentration of CNTs is by the magnetic susceptibility of the ferrocene present in the CNTs by the synthesis process, which can be performed on sample coupons on a vibrating sample magnetometer (VSM); VSM is a bulky laboratory instrument, and the size of the samples studied is constrained. In order to provide a technique that is fast, easy, cheap, and adaptable to the size of the samples, we have developed a benchtop device that measures the CNT concentration through an original inductive dynamic measurement of the ferrocene magnetic susceptibility. We present the method for extracting CNT concentrations and show the results obtained on cement matrices with CNT concentrations of the order of a few percent.
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http://dx.doi.org/10.1063/5.0161197 | DOI Listing |
Turk J Chem
November 2024
School of Chemical and Blasting Engineering, Anhui University of Science and Technology, Huainan, P.R. China.
The development of ultraviolet (UV) shielding materials is of great importance to protect human health and prevent the degradation of organic matter. However, the synthesis of highly efficient UV shielding polymer nanocomposites is currently limited by the agglomeration of inorganic anti-UV nanoparticles (NPs) within the polymer matrix and the limited absorption spectrum of UV shielding agents. In this study, highly effective manganese doped carbon quantum dots@halloysite nanotube composites (Mn-CDs@HNTs/PAS) were successfully synthesized by loading manganese-doped carbon quantum dots (Mn-CDs) into UV shielding effective halloysite nanotubes (HNTs) via the solvothermal method, followed by polymerization modification (PAS).
View Article and Find Full Text PDFSmall
January 2025
College of Chemistry, Chemical Engineering and Materials Science, Soochow University, Suzhou, Jiangsu, 215123, China.
Bio-inspired by tactile function of human skin, piezoionic skin sensors recognize strain and stress through converting mechanical stimulus into electrical signals based on ion transfer. However, ion transfer inside sensors is significantly restricted by the lack of hierarchical structure of electrode materials, and then impedes practical application. Here, a durable nanocomposite electrode is developed based on carbon nanotubes and graphene, and integrated into piezoionic sensors for smart wearable applications, such as facial expression and exercise posture recognitions.
View Article and Find Full Text PDFBMC Chem
January 2025
National Organization for Drug Control and Research (NODCAR), P.O.Box 29, Cairo, Egypt.
Tirofiban hydrochloride is used to inhibit platelet aggregation, which has a significant impact on the treatment of congestive heart failure the most common cause of death according to WHO. Therefore, its quantification in pharmaceutical dosage form is critical. In this work, an electrochemical method for the determination of tirofiban HCl in pharmaceutical dosage form was developed and validated.
View Article and Find Full Text PDFSci Rep
January 2025
Department of Physics, Faculty of Science, Vali-e-Asr University of Rafsanjan, Rafsanjan, Iran.
To protect against harmful electromagnetic interference (EMI), it is crucial to fabricate composite with high total electromagnetic shielding efficiency (SE); In this study, FeNi-NiFeO-SiO nanoparticles (NPs) were synthesized using one-pot method and decorated on carbon nanotube's (CNT) sidewall. The final product was magnetic-ceramic/conductive (FeNi-NiFeO-SiO/MWCNT) nanocomposite. The EMI shielding characteristic of FeNi-NiFeO-SiO NPs and FeNi-NiFeO-SiO/MWCNT nanocomposite was investigated in the range of X and Ku frequency band.
View Article and Find Full Text PDFCarbohydr Polym
March 2025
Beijing Key Laboratory of Lignocellulosic Chemistry, MOE Engineering Research Center of Forestry Biomass Materials and Energy, Beijing Forestry University, Beijing 100083, China; State Key Laboratory of Efficient Production of Forest Resources, Beijing 100083, China. Electronic address:
Integrating liquid metal (LM) with wood fibers for flexible paper electronics is intriguing yet extremely challenging due to poor mechanical performance. Here, we disclose a hemicellulose trapping strategy to achieve exceptional ultrastrong and tough LM-based paper electronics. Holocellulose nanofibrils (HCNFs) with hemicellulose retention of approximately 20 % are found to effectively entrap nanoscale LM within the fibril network, analogous to spider silk capturing small water droplets.
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