Trivalent chromium ion-activated broadband near-infrared (NIR) luminescence materials have shown great application prospects as next-generation NIR light sources, but improvement of the luminescence efficiency remains a challenge. Herein, novel KLiScF:Cr and KLiScF:Cr/Mn broadband fluoride NIR phosphors are designed and prepared by a combination of hydrothermal and cation exchange methods for the first time. The crystal structure and photoluminescence (PL) properties of KLiScF:Cr are studied in detail, which shows strong absorption in the blue light region ( = 432 nm) and broadband NIR emission ( = 770 nm) with a PL quantum efficiency of 77.6%. More importantly, the NIR emission of Cr can be enhanced by co-doping with Mn, which may provide an alternative way for improving the PL intensity of Cr-activated broadband NIR phosphors. Finally, a NIR phosphor-converted LED (pc-LED) device is fabricated using the as-prepared NIR phosphor and its application in bio-imaging and night vision has been evaluated.
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