A penta-stranded helicate was obtained by combining [Pd(CHCN)](BF) with La(NO) and a polydentate ligand. The helicate displays low symmetry, both in solution and in the solid state. A dynamic interconversion between the penta-stranded helicate and a symmetrical, four-stranded helicate was achieved by adjustment of the metal-to-ligand ratio.
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A five-stranded heterometallic helicate.
Chem Commun (Camb)
June 2023
Institut of Chemical Sciences and Engineering, Ecole Polytechnique Fédérale de Lausanne (EPFL), Lausanne 1015, Switzerland.
A penta-stranded helicate was obtained by combining [Pd(CHCN)](BF) with La(NO) and a polydentate ligand. The helicate displays low symmetry, both in solution and in the solid state. A dynamic interconversion between the penta-stranded helicate and a symmetrical, four-stranded helicate was achieved by adjustment of the metal-to-ligand ratio.
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