The tests discussed in the article aimed to analyse the structure and hardness of the heat affected zone and that of the weld in thin butt joints (1.0 mm) made of Inconel 718 using the TIG method and variable welding linear energy restricted within the range of 45 J/mm to 80 J/mm. The test joints were subjected to visual tests, macro and microscopic metallographic tests, scanning electron microscopy-based structural observations and hardness measurements. The tests concerned with the effect of the TIG welding of butt joints made of 1.0 mm thick sheets (Inconel 718) in laboratory conditions revealed that the most favourable quality of the sheets was obtained when welding arc linear energy was restricted within the range of approximately 45 J/mm to 80 J/mm. An increase in linear energy within the above-presented range led to an increase in the width of the weld and that of the HAZ (observed in the joints subjected to macroscopic metallographic tests). In addition, an increase in linear energy restricted within the aforesaid range increased the grain size in matrix γ (in the HAZ) from approximately 10 μm-20 μm. The structure of the weld contained the zone of columnar grains oriented towards the fusion line as well as large groups of primary grains having the dendritic structure with clearly visible axes of primary dendrites of varied orientation. In addition, the weld structure also contained precipitates in the form of low-melting eutectics located in interdendritic spaces.
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http://dx.doi.org/10.1016/j.heliyon.2023.e13175 | DOI Listing |
Pest Manag Sci
January 2025
Institute of Mechanical, Process & Energy Engineering., Heriot-Watt University, Edinburgh, UK.
Background: Identifying robust integrated pest management (IPM) strategies requires the testing of multiple factors at the same time and assessing their combined effects e.g., on disease control.
View Article and Find Full Text PDFChem Sci
January 2025
School of Chemistry and Chemical Engineering, Shandong University 250100 Jinan China
Understanding the adsorption behavior of intermediates at interfaces is crucial for various heterogeneous systems, but less attention has been paid to metal species. This study investigates the manipulation of Co spin states in ZnCoO spinel oxides and establishes their impact on metal ion adsorption. Using electrochemical sensing as a metric, we reveal a quasi-linear relationship between the adsorption affinity of metal ions and the high-spin state fraction of Co sites.
View Article and Find Full Text PDFHeliyon
January 2025
Environmental Health Research Center, Research Institute for Health Development, Kurdistan University of Medical Sciences, Sanandaj, Iran.
In this study, a Cu@Ag core-shell was synthesized using a co-precipitation method. To create a new electrochemical sensor, a Cu@Ag core-shell with conductive polymers such as polyalizarin yellow R (PA) and Nafion (Nf) was immobilized on the surface of a glassy carbon electrode (Cu@Ag-Nf/PA/GCE). X-ray diffraction analysis (XRD), energy dispersive X-ray analysis (EDX), transmission electron microscopy (TEM), and Fourier Transform Infrared Spectroscopy (FTIR) techniques were employed to characterize the Cu@Ag-Nf/PA/GCE.
View Article and Find Full Text PDFIndian J Nucl Med
November 2024
Center for Research and Production of Radioisotopes, Dalat Nuclear Research Institute, Vietnam Atomic Energy Institute (VINATOM), Da Lat City, Lam Dong Province, Vietnam.
Aims: This study aimed to evaluate the principal technical characteristics of a well-type gas-filled ionization chamber dose calibrator used in measuring radiopharmaceutical activity, namely accuracy, repeatability, and linearity. Furthermore, this work also explored the correlation between the device's response and the position and volume of the radiopharmaceutical I-131.
Materials And Methods: Experimental measurements were conducted on the ATOMLAB 500 dose calibrator using NIST traceable Cs-137 source to determine the accuracy and repeatability.
Nano Lett
January 2025
College of Energy, Xiamen University, Xiamen 361102, China.
The optimized composition and precisely tailored structure configuration play critical roles in enhancing the catalytic reaction kinetics. Here we report a distinctive core@satellite strategy for designing the advanced platinum-nickel@platinum-nickel-copper-cobalt-indium high-entropy alloy nanowires (PtNi@HEA NWs) as efficient bifunctional catalysts in the proton exchange membrane fuel cell. Impressively, the PtNi@HEA NWs/C shows 19.
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