The title compound, CHO, is formed as the major product from the reaction between -1,2-bis-(pinacolatoboron)-1,2-bis-(4-methyl-carb-oxy-phen-yl)ethene and excess methyl 4-iodo-benzoate in basic DMSO using a palladium catalyst at 80°C Suzuki coupling followed by protodeboronation. Crystals were grown by slow evaporation of a hexa-nes solution at room temperature.
Download full-text PDF |
Source |
---|---|
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462201 | PMC |
http://dx.doi.org/10.1107/S2414314620004174 | DOI Listing |
Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!