The title compound, CHO, is formed as the major product from the reaction between -1,2-bis-(pinacolatoboron)-1,2-bis-(4-methyl-carb-oxy-phen-yl)ethene and excess methyl 4-iodo-benzoate in basic DMSO using a palladium catalyst at 80°C Suzuki coupling followed by protodeboronation. Crystals were grown by slow evaporation of a hexa-nes solution at room temperature.

Download full-text PDF

Source
http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9462201PMC
http://dx.doi.org/10.1107/S2414314620004174DOI Listing

Publication Analysis

Top Keywords

trimethyl 44'4''-ethene-112-tri-yltribenzoate
4
44'4''-ethene-112-tri-yltribenzoate title
4
title compound
4
compound cho
4
cho formed
4
formed major
4
major product
4
product reaction
4
reaction -12-bis-pinacolatoboron-12-bis-4-methyl-carb-oxy-phen-ylethene
4
-12-bis-pinacolatoboron-12-bis-4-methyl-carb-oxy-phen-ylethene excess
4

Similar Publications

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!