Effect of zirconium oxide nano-coating on frictional resistance of orthodontic wires.

Objectives: Minimizing the frictional force between orthodontic wire and brackets is imperative to safely obtain a more favorable result by applying lower loads. Several methods have been proposed for this purpose such as changing the wire shape/size, changing the bracket design, and coating wires with different materials. This study aimed to assess the effect of zirconium oxide (ZrO2) nano-coating on frictional resistance of three types of orthodontic wires.

Materials And Methods: This in vitro, experimental study evaluated 42 pieces of nickel-titanium (NiTi), stainless steel (SS), and beta-titanium (TMA) orthodontic wires, and 42 maxillary canine brackets. The samples were divided into six groups with and without ZrO2 nano-coating. The nano-coating was applied on the wires using the sol-gel technique. The presence of ZrO2 nano-coating was evaluated by scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX). The surface roughness of the samples was evaluated using atomic force microscopy (AFM). The brackets and wire had a 5° angle relative to each other. The static and kinetic friction of the samples were evaluated in the presence of artificial saliva and occlusogingival movements in a universal testing machine. Data were analyzed by the Shapiro-Wilk's test, one-way ANOVA, Kruskal-Walli's test, Mann-Whitney U test, independent t-test, and Tukey's test.

Results: ZrO2 nano-coating was only observed on TMA wires. The surface roughness of coated NiTi and SS wires had no significant difference from that of non-coated wires ( > 0.05). However, this difference was significant for TMA wires with and without the coating ( < 0.05). The static and kinetic friction were not significantly different between wires with and without coating ( > 0.05).

Conclusions: ZrO2 nano-coating could only be applied on TMA wires, and had no significant efficacy for reduction of static or kinetic friction of TMA wires.