A Pd-catalyzed borylsilylative cyclization of 1,6-allenynes with PhMeSiBpin was developed. This method provides a practical and general method to afford the carbocycles and heterocycles bearing silyl and boryl groups with excellent regioselectivities and stereoselectivities in high to excellent yields.
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Pd-Catalyzed Borylsilylative Cyclization of 1,6-Allenynes.
Org Lett
September 2022
NMPA Key Laboratory for Research and Evaluation of Innovative Drug, Henan Key Laboratory of Organic Functional Molecule and Drug Innovation, School of Chemistry and Chemical Engineering, Henan Normal University, Xinxiang, Henan 453007, P. R. China.
A Pd-catalyzed borylsilylative cyclization of 1,6-allenynes with PhMeSiBpin was developed. This method provides a practical and general method to afford the carbocycles and heterocycles bearing silyl and boryl groups with excellent regioselectivities and stereoselectivities in high to excellent yields.
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