Bonding of Resin Cements to Ultra-Translucent Zirconia After Aging for 24 Hours and 1 Year.

Purpose: To evaluate the effect of different luting techniques on the shear bond strength (SBS) of ultra-translucent multi-layered zirconia (UTML) after 24 hours and 1 year of water storage and to analyze the influence of primers on the wettability of the UTML MTU-6 surface.

Materials And Methods: Four commercial resin cements were evaluated: Variolink Esthetic LC (Ivoclar Vivadent); RelyX Ultimate (3M); Estecem II (Tokuyama); and Panavia V5 (Kuraray Noritake). Panavia V5 was tested with and without Panavia V5 Tooth Primer (Kuraray Noritake). The SBS immediately after cement/primer application and after aging, scanning electron microscopy of the surfaces, and the contact angle of the primers on the UTML surfaces were analyzed.

Results: At 24 hours, Panavia V5 with Tooth Primer exhibited the highest SBS. After 1 year, the SBS of Variolink Esthetic LC and Panavia V5 with Tooth Primer decreased, and RelyX Ultimate increased. There was no statistical difference between RelyX Ultimate and Panavia V5 with Tooth Primer at 1 year. For all groups, the rate of adhesive failures increased after 1 year. The highest contact angle was observed on the control (no primer) group, and the lowest contact angles were obtained when the YSZ surface was treated with Scotchbond Universal and the combination of Clearfil Ceramic Primer Plus and Tooth Primer.

Conclusion: Clinicians should prefer 10-MDP-based cementation systems that can be properly polymerized to achieve a stable long-term bond strength to YSZ restorations. Also, the use of ceramic primers improves the capability of the cement to establish an intimate contact with the intaglio of the restoration.