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Cadmium-rich intermetallic phases RhCd - structure, magnetic behavior, Eu Mössbauer and Cd solid-state NMR spectroscopy.
Dalton Trans
January 2025
Institut für Anorganische und Analytische Chemie, Universität Münster, Corrensstraße 30, 48149 Münster, Germany.
The cadmium-rich intermetallic compounds RhCd ( = Ca, Sr, Y, La-Nd, Sm-Lu) were synthesized from the elements in sealed tantalum tubes. The elements were reacted in an induction furnace and the samples were post-annealed to increase phase purity and crystallinity. The RhCd phases crystallize with the cubic CeCrAl type structure, space group 3̄.
View Article and Find Full Text PDFMammals in urban centers: a dataset from the perspective of the media in Brazil.
Zookeys
January 2025
Laboratório de Ecologia e Biogeografia de Mamíferos, Universidade Estadual de Goiás, Avenida Brasil, Setor Helio Leao, Quirinópolis, GO, Brazil Universidade Estadual de Goiás Quirinópolis Brazil.
The continuous growth of the urban population, coupled with habitat loss, has resulted in unanticipated interactions between animals and humans in urban centers. In this study, we investigated the presence of mammals in urban centers through newspaper reports on websites. Specifically, we examined: i) the frequency of photographic records, ii) the temporal trends (2001 to 2021) and spatial trends (Brazilian Federative regions and states) of the records, and iii) the orders, families, and species most frequently reported in urban centers.
View Article and Find Full Text PDFIGF-1 Assessment During Weekly Somatrogon Treatment in Pediatric Patients With GH Deficiency.
J Endocr Soc
January 2025
Pfizer Inc, Collegeville, PA 19426, USA.
Context: In patients with GH deficiency (GHD) receiving GH treatment, IGF-1 concentrations are used by physicians to monitor treatment safety and efficacy and guide dosing decisions. Somatrogon is a long-acting GH approved as a once-weekly treatment for pediatric GHD. Somatrogon administration results in characteristic changes in the IGF-1 profile, with values measured at 96 hours postdose representing mean IGF-1 concentrations that best reflect overall somatrogon exposure.
View Article and Find Full Text PDFSequential separation of anti-diabetic drugs in the presence of melamine as impurity using chromatographic methods.
BMC Chem
January 2025
Pharmaceutical Chemistry Department, Faculty of Pharmacy, Nahda University, Sharq El-Nile, Beni-Suef, 62511, Egypt.
The study of green analytical chemistry has garnered significant attention in the context of mitigating global environmental contamination. In this study, we present two methodologies for environmentally friendly chromatography that enable simultaneous and specific determination of Saxagliptin (SAX), metformin (MET), and a pharmacopoeial impurity of MET known as melamine (MEL). The initial method employed in this study is High-Performance Thin Layer Chromatography (HPTLC), which utilized 60 F 254 silica gel-coated Mark HPTLC plates on aluminum sheets as the stationary phase.
View Article and Find Full Text PDFState-dependent neurovascular modulation induced by transcranial ultrasound stimulation.
Med Biol Eng Comput
January 2025
School of Biomedical Engineering, Shanghai Jiao Tong University, No.1954 Huashan Road, Shanghai, 200030, Shanghai, China.
Previous studies reported baseline state-dependent effects on neural and hemodynamic responses to transcranial ultrasound stimulation. However, due to neurovascular coupling, neither neural nor hemodynamic baseline alone can fully explain the ultrasound-induced responses. In this study, using a general linear model, we aimed to investigate the roles of both neural and hemodynamic baseline status as well as their interactions in ultrasound-induced responses.
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