The complexity of biaxial tests and analysis of their results makes it difficult to study the interlaminar shear properties of fibre-reinforced composites, particularly under through-thickness compression, which occurs in thick-walled composite elements. The improvements in experimental methods to study the features of the nonlinear behaviour of composites under biaxial loading is now an important and relevant task in the development aircraft structural elements made of carbon fibre-reinforced polymers. This study aimed to develop a new experimental approach for the reliable determination of the interlaminar shear properties of laminates under through-thickness compression using a standard testing machine. An appropriate V-notched specimen was developed based on the configuration of well-known Iosipescu and butterfly-shaped specimens. The approach is demonstrated using woven carbon/epoxy laminates. Both the preliminary assessment of the stress fields under combined compression/shear loading and the analysis of fracture mechanisms were performed with finite-element modelling in a three-dimensional formulation. The digital image correlation (DIC) method was used to obtain experimental, full-field deformations of the specimens and to estimate the uniformity of the strain distribution in the gauge section. The stress-strain curves were obtained under biaxial loading, and the corresponding features of the composite failure behaviour were analysed in detail. It was found that the maximum compression strain on the stress-strain curves, in some cases, corresponded to the discontinuity in the composite structure. In these cases, the disproportionate changes in through-thickness strains in the gauge section of the specimens were recorded at the maximum load. With the increase in through-thickness compression stresses, the difference between the shear strength values, determined by the maximum load and the maximum compressive strain, increased by up to 20%. It was shown that the assessment of the composite strength at maximum load at the design stage significantly increased the risk of premature failure of the composite elements during exploitation.
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http://dx.doi.org/10.3390/polym14132575 | DOI Listing |
Materials (Basel)
December 2024
AVIC Manufacturing Technology Institute Composite Technology Center, Beijing 101300, China.
Carbon fiber (CF)-reinforced polyimide (PI) resin matrix composites have great application potential in areas such as rail transport, medical devices, and aerospace due to their excellent thermal stability, dielectric properties, solvent resistance, and mechanical properties. However, the epoxy sizing agent used for traditional carbon fiber cannot withstand the processing temperature of polyimide resin, of up to 350 °C, resulting in the formation of pores or defects at the interface between the fiber and the resin matrix, leading to the degradation of the overall composite properties. To overcome this problem, in this study, a low-molecular-weight thermosetting polyimide sizing agent was prepared and the processability of the sized carbon fiber was optimized by a thermoplastic polyimide.
View Article and Find Full Text PDFPolymers (Basel)
December 2024
Institute of Catalysis for Energy and Environment, College of Chemistry and Chemical Engineering, Shenyang Normal University, Shenyang 110136, China.
Interlaminar shear strength (ILSS) and compressive strength are two of the most critical properties of carbon fiber-reinforced polymer (CFRP). In this report, three types of epoxy resins-4,4'-diaminodiphenylmethane epoxy resin (AG-80), bisphenol A epoxy resin (E-1NT), and novolac epoxy (EPN)-were studied. E-1NT is characterized by low viscosity and low cost but exhibits poor mechanical properties, while AG-80 offers better wetting with carbon fiber.
View Article and Find Full Text PDFInt J Biol Macromol
December 2024
School of Materials Science and Engineering, Shandong University of Science and Technology, 266590 Qingdao, China. Electronic address:
Polymers (Basel)
October 2024
Department of Materials, Textiles and Chemical Engineering (MATCH), Ghent University, Technologiepark 907, B-9052 Zwijnaarde, Belgium.
This study investigates the effectiveness of polyether block amide (PEBA) thermoplastic elastomeric nanofibers in reducing low-velocity impact damage across three carbon fiber composite lay-up configurations: a cross-ply [0°/90°]2s (CP) and a quasi-isotropic [0°/45°/90°/-45°]s (QI) lay-up utilizing unidirectional plies, and a stacked woven [(0°,90°)]4s (W) lay-up using twill woven fabric plies. The flexural strength and interlaminar shear strength of the composites remained unaffected by the addition of nanofibers: around 750 MPa and 63 MPa for CP, 550 MPa and 58 MPa for QI, and 650 MPa and 50 MPa for W, respectively. The incorporation of nanofibers in the interlaminar regions resulted in a substantial reduction in projected damage area, ranging from 30% to 50% reduction over an impact energy range of 5-20 J.
View Article and Find Full Text PDFMaterials (Basel)
September 2024
Key Laboratory for Liquid Solid Structural Evolution and Processing of Materials (Ministry of Education), School of Materials Science and Engineering, Shandong University, Jinan 250061, China.
In this study, vinyltriethoxysilane (TEVS) was introduced onto the surface of carbon fiber using liquid-phase oxidation and impregnation methods to incorporate vinyl groups onto the carbon fiber, thereby enhancing the chemical bonding between the carbon fiber and norbornene-polyimide (PI-NA). Through a systematic study of the hydrolysis conditions and concentration of the TEVS solution, the optimal modification conditions were determined. These conditions were used to graft TEVS onto the surface of oxidized carbon fiber to prepare carbon-fiber-reinforced PI-NA composites (CF/PI-NA).
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