A catalyzed process for the synthesis of the 4,6-substituted 3,4-dihydro-1,3-oxazin-2-one skeleton has been developed through cycloaddition of generated acyliminium intermediates with alkynes. A range of chain ,-acetals and terminal alkynes were amenable for this mild transformation. As a result, a series of desired cycloaddition products were obtained in moderate to good yields.
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| http://dx.doi.org/10.1039/d2ob00900e | DOI Listing |
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