The alkaloid profile of L. and subsp. (Kreyer) Avet have not been characterized yet. UHPLC-PDA-Q-TOF-MS/MS and LC-DAD-QqQ-MS/MS methods were used herein to characterize the metabolite profiles of these plants. Flash chromatography in combination with preparative- and semi preparative HPLC were utilized for the isolation of the compounds of interest. The structure of the isolated compounds was proposed based on their MS/MS fragmentation and NMR characteristics. As a total of 19 tropane derivatives, two tyramine derivatives (-- and -- feruloyl tyramine), a lignanamide (grossamide), an alkylamide (pellitorine) were identified in the root and herb extracts of . Moreover, rutin and caffeoylquinic acids were found in the leaves and fruits, while kaempferol-3--glucoside-7--rhamnoside and quercetin-3--glucoside-rhamnoside-rhamnoside were exclusively characteristic for the leaves of . The root and herb extracts of contained 16 tropane alkaloid derivatives along with methyl tropate and two tyramine derivatives.
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