An efficient protocol for synthesis of thioamides was developed the microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines. This process is scalable and tolerates a wide spectrum of amines to deliver the corresponding products in moderate to excellent yields in 10 minutes, providing a cheap and rapid approach to thioamides.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9070997 | PMC |
| http://dx.doi.org/10.1039/c9ra05939c | DOI Listing |
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Microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines: a rapid and efficient protocol for thioamides.
RSC Adv
September 2019
Institution of Functional Organic Molecules and Materials, School of Chemistry and Chemical Engineering, Liaocheng University No. 1, Hunan Street Liaocheng Shandong 252059 P. R. China.
An efficient protocol for synthesis of thioamides was developed the microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines. This process is scalable and tolerates a wide spectrum of amines to deliver the corresponding products in moderate to excellent yields in 10 minutes, providing a cheap and rapid approach to thioamides.
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