An efficient continuous flow sequential synthesis of diaryl ketones was achieved by coupling of aryl Grignard reagents with acyl chlorides in the bio-derived "green" solvent 2-methyltetrahydrofuran (2-MeTHF) under mild reaction conditions (ambient temperature, 1 hour), allowing a safe and on-demand generation of 2-(3-benzoylphenyl)propionitrile with a productivity of 3.16 g hour.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC9059842 | PMC |
| http://dx.doi.org/10.1039/c8ra07447j | DOI Listing |
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