[Rapid determination of 30 volatile organic compounds in workplace air by gas chromatography].

Zhonghua Lao Dong Wei Sheng Zhi Ye Bing Za Zhi

Inspection and Testing Department, Changxing Center for Disease Control and Prevention, Huzhou 313100, China.

Published: March 2022

To establish a method for rapid detection of DB-WAX capillary column and determination of the workplace air in 30 kinds of volatile organic pollutants. In August 2020, N-pentane, n-hexane, methylcyclohexane, octane, Acetone, ethyl acetate, butanone, benzene, 3-pentanone, trichloroethylene, tetrachloroethylene, toluene, butyl acetate, 2-hexanone, Isoamyl acetate, ethylbenzene, p-xylene, m-xylene, amyl acetate, o-xylene, chlorobenzene, styrene, cyclohexanone, P-chlorotoluene, bromobenzene, M-dichlorobenzene, p-dichlorobenzene, O-dichlorobenzene, o-Chlorotoluene, 1, 2 , 4-trichlorobenzene of 30 kinds of substances in air were collected by activated carbon tube. After analysis by carbon disulfide, the analytical solution was analyzed by DB-WAX column and determined by FID detector. The above 30 kinds of volatile organic pollutants had good separation effect, the correlation coefficient of the standard curve was above 0.999, the relative standard deviation was 0.1%-3.2%, the desorption efficiency was 77.0%-117.1% , the lower limit of quantitation was 0.33-5.33 μg/ml, and the lowest quantitation concentration was 0.22-3.55 mg/m(3), the recoveries ranged was 95.4%-104.9%. The method can effectively separate and accurately determine 30 volatile organic compounds in these workplaces, and the method is simple and quick.

Download full-text PDF

Source
http://dx.doi.org/10.3760/cma.j.cn121094-20201217-00697DOI Listing

Publication Analysis

Top Keywords

volatile organic
16
organic compounds
8
workplace air
8
kinds volatile
8
organic pollutants
8
[rapid determination
4
volatile
4
determination volatile
4
organic
4
compounds workplace
4

Similar Publications

Enhancing beer authentication, quality, and control assessment using non-invasive spectroscopy through bottle and machine learning modeling.

J Food Sci

January 2025

Digital Agriculture, Food and Wine Research Group, School of Agriculture, Food and Ecosystem Science, Faculty of Science, The University of Melbourne, Melbourne, Victoria, Australia.

Fraud in alcoholic beverages through counterfeiting and adulteration is rising, significantly impacting companies economically. This study aimed to develop a method using near-infrared (NIR) spectroscopy (1596-2396 nm) through the bottle, along with machine learning (ML) modeling for beer authentication, quality traits, and control assessment. For this study, 25 commercial beers from different brands, styles, and three types of fermentation were used.

View Article and Find Full Text PDF

Introduction: Breath Volatile organic compounds (VOCs) are promising biomarkers for clinical purposes due to their unique properties. Translation of VOC biomarkers into the clinic depends on identification and validation: a challenge requiring collaboration, well-established protocols, and cross-comparison of data. Previously, we developed a breath collection and analysis method, resulting in 148 breath-borne VOCs identified.

View Article and Find Full Text PDF

Monitoring persistent organic pollutants (POPs) with endocrine-disrupting properties poses significant analytical challenges due to labor-intensive, costly, and environmentally unsustainable procedures. This study developed an efficient and robust approach for the simultaneous detection of diverse groups of semi-volatile organics in water and sediment samples using gas chromatography-tandem mass spectrometry (GC-MS). Two extraction methods were studied for determining POPs in water and sediments.

View Article and Find Full Text PDF

Modulating the electronic structure of noble metals via electronic metal-support interaction (EMSI) has been proven effectively for facilitating molecular oxygen activation and catalytic oxidation reactions. Nevertheless, the investigation of the fundamental mechanisms underlying activity enhancement has primarily focused on metal oxides as supports, especially in the catalytic degradation of volatile organic compounds. In this study, a novel Pt catalyst supported on nitrogen-doped carbon encapsulating FeNi alloy, featuring ultrafine Pt nanoparticles, was synthesized.

View Article and Find Full Text PDF

Changes in key volatile components associated with leaf quality of Roxb. alongside growth duration.

Food Chem X

January 2025

Spice and Beverage Research Institute, Chinese Academy of Tropical Agricultural Sciences/ Hainan Provincial Key Laboratory of Genetic Improvement and Quality Regulation for Tropical Spice and Beverage Crops/ Key Laboratory of Genetic Resource Utilization of Spice and Beverage Crops, Ministry of Agriculture and Rural Affairs, Wanning, Hainan 571533, China.

Pandan ( Roxb.) are one of the traditional food materials in Southeast Asian countries. However, there has long been a lack of understanding of the differences in volatile organic compounds (VOCs) of leaves at different growth periods.

View Article and Find Full Text PDF

Want AI Summaries of new PubMed Abstracts delivered to your In-box?

Enter search terms and have AI summaries delivered each week - change queries or unsubscribe any time!