Nano-[FeO@SiO/-propyl-1-(thiophen-2-yl)ethanimine][ZnCl] as a nano magnetite Schiff base complex was designed and fully characterized by various analyses such as Fourier transform infrared spectroscopy (FT-IR), energy-dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), thermal gravimetric analysis (TGA), differential thermal gravimetric analysis (DTA), vibrating sample magnetometry (VSM), scanning electron microscopy (SEM), and transmission electron micrographs (TEM). The presented nano magnetite Schiff base complex was used as a heterogeneous catalyst for the synthesis of pyrimido[4,5-]quinolones by the reaction of aryl aldehyde, dimedone and 6-amino-1,3-dimethyluracil in EtOH : HO (7 : 3) as a solvent at 60 °C.
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http://dx.doi.org/10.1039/d2ra00213b | DOI Listing |
Acc Chem Res
January 2025
Institute of Energy: Sustainability, Environment and Equity (I:SEE), State University of New York at Stony Brook, Stony Brook, New York 11794, United States.
ConspectusLithium-ion batteries are recognized as an important electrochemical energy storage technology due to their superior volumetric and gravimetric energy densities. Graphite is widely used as the negative electrode, and its adoption enabled much of the modern portable electronics technology landscape. However, developing markets, such as electric vehicles and grid-scale storage, have increased demands, including higher energy content and a diverse materials supply chain.
View Article and Find Full Text PDFSci Total Environ
January 2025
Department of Electroceramics and Electrical Engineering, Malek Ashtar University of Technology, Iran.
As a primary abiotic constraint for bean cultivation in semi-arid regions, drought stress significantly impacts both the yield and quality of beans. Foliar application of nanofertilizer has been shown to effectively improve crop yield and nutritional quality while mitigating environmental pollution associated with fertilizer runoff. In this study, we conducted a semi-field study using magnetite nanoparticles (FeONPs) to evaluate its effects on the growth, yield, nutrient quality, photosynthetic parameters, and physiological traits in kidney bean (Phaseolus vulgaris L.
View Article and Find Full Text PDFImpact of climate change that stems from gaseous emissions require sustainable materials to eliminate sulfur. This study involves the modification of humic acid with magnetite nanoparticles (Fe₃O₄ NPs) by a microwave-assisted synthesis of an absorbent with reasonable pore volume and diameter for elimination of thiophenic compounds from fuel. The magnetic nano adsorbent designated Fe3O4@HA was characterized using advanced spectroscopic techniques, while their structure and morphology were analyzed through DLS, XPS, XRD, FT-IR, TGA, FESEM-EDX, VSM, and BET-N2 techniques.
View Article and Find Full Text PDFMikrochim Acta
January 2025
Shanxi Key Laboratory of Micro Nano Sensors & Artificial Intelligence Perception, College of Integrated Circuits, Taiyuan University of Technology, Taiyuan, 030024, China.
African swine fever (ASF) is an acute hemorrhagic disease in pigs caused by the African swine fever virus (ASFV), which has a high mortality rate and brought great damage to global pig farming industry. At present, there is no effective treatment or vaccine to combat ASFV infection, so early detection of ASFV has become particularly important. Therefore, the PDMS/chitosan/MPMs composite film was proposed to detect ASFV P72.
View Article and Find Full Text PDFDiscov Nano
January 2025
Particle Engineering Centre, Department of Chemical Engineering, Norwegian University of Science and Technology, Trondheim, 7491, Norway.
The increasing demand for magnetic iron oxide nanoparticles (IONPs) in biomedicine necessitates efficient and scalable production methods. Thermal decomposition offers excellent tailoring of the particle properties but its discontinuous batch-operation is restricting scale-up and industrial application. To overcome these challenges, several studies have demonstrated semi-continuous thermal decomposition by slowly injecting the precursor, though only half of them produce magnetite IONPs and even fewer use iron oleate precursors.
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