Ceramic flash sintering with a strong electric field at room temperature is the most attractive method. This paper presents the flash sintering of ZnO ceramics at room temperature by the application of a 3-kV/cm electric field after a dropwise addition of ethanol. This method is simple and easy to control. The density of the specimen exceeded 96% after 30 s of sintering. No significant difference was observed in the initiation voltage of flash sintering with and without the dropwise addition of ethanol. Ethanol burns upon dropwise addition, causing a discharge to first occur far from the location of the dropwise addition, followed by glowing and heating up, which causes the temperature of the entire specimen to rise.
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http://dx.doi.org/10.3390/ma15030862 | DOI Listing |
ACS Nano
January 2025
Division of Advanced Nano-Materials, Suzhou Institute of Nano-Tech and Nano-Bionics, Chinese Academy of Sciences, Suzhou 215123, China.
Heating techniques have underpinned the progress of the material and manufacturing industries. However, the explosive development of nanomaterials and micro/nanodevices has raised more requirements for the heating technique, including but not limited to high efficiency, low cost, high controllability, good usability, scalability, universality, and eco-friendliness. Carbothermal shock (CTS), a heating technique derived from traditional electrical heating, meets these requirements and is advancing at a high rate.
View Article and Find Full Text PDFACS Nano
September 2024
Department of Mechanical Convergence Engineering, Hanyang University, 222 Wangsimni-ro, Seongdong-gu, Seoul 04763, Republic of Korea.
This study focused on addressing the challenges associated with the incompatibility between sulfide solid electrolytes and Ni-rich cathode active materials (CAMs) in all-solid-state lithium-ion batteries. To resolve these issues, protective layers have been explored for Ni-rich materials. Lithium lanthanum titanate (LLTO), a perovskite-type material, is recognized for its excellent chemical stability and ionic conductivity, which render it a potential protective layer in CAMs.
View Article and Find Full Text PDFNanoscale
July 2024
National & Local Joint Engineering Research Center of Semiconductor Display and Optical Communication Devices, South China University of Technology, Guangzhou 510641, China.
Compared to conventional heating techniques, the carbon carrier-based rapid Joule heating (CJH) method is a new class of technologies that offer significantly higher heating rates and ultra-high temperatures. Over the past few decades, CJH technology has spawned several techniques with similar principles for different application scenarios, including ultra-fast high temperature sintering (UHS), carbon thermal shock (CTS), and flash Joule heating (FJH), which have been widely used in material preparation research studies. Functional nanomaterials are a popular direction of research today, mainly including nanometallic materials, nanosilica materials, nanoceramic materials and nanocarbon materials.
View Article and Find Full Text PDFNanomaterials (Basel)
March 2024
Institute of Materials Science and Technology, TU Wien, Getreidemarkt 9, 1060 Vienna, Austria.
The thermodynamic and kinetic simulations based on the re-assessment of the thermodynamic and kinetic database of the Ni-Ti-Cu system were employed to predict the phenomena of mechanical alloying, spark plasma sintering and thermal properties of the intriguing Ni-Ti-Cu system. Thermodynamic calculations are presented for the stable and unstable phases of NiTiCu materials and support a correlation with the evolving microstructure during the technological process. Also, the thermal conductivity, the thermal diffusivity and the specific heat of spark plasma sintered and aged Cu-alloyed NiTi-based shape memory alloys (NiTiCu) with two compositions, NiTiCu and NiTiCu, are evaluated and the influence of mechanical alloying and precipitates on thermal properties is discussed.
View Article and Find Full Text PDFInt J Biol Macromol
February 2024
Department of Metallurgical Engineering and Materials Science, Indian Institute of Technology Bombay, Mumbai, Maharashtra 400076, India. Electronic address:
Real-time monitoring of low temperatures (usually below 0 °C) or cold environments is a specific requirement that finds its high demand in the aerospace, pharmaceutical, food, and beverage industries to maintain the temperature at high altitudes or in refrigerators and cold storage. In general, this purpose is achieved by using a sub-zero temperature sensor coupled with a control system. However, the market available such temperature sensors are very expensive, and bulky, thus not being suitable for portable operation, and also they suffer from poor accuracy.
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