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Synthesis and crystal structure of a solvated Co complex with 2-hy-droxy-3-meth-oxy-benzaldehyde thio-semicarbazone ligands. | LitMetric
The title Co complex, bis-[bis-(2-hy-droxy-3-meth-oxy-benzaldehyde thio-semi-carbazonato)cobalt(III)] di-thio-nate-dimethylformamide-methanol (1/4/3), [Co(CHNOS)](SO)·4CHNO·3CHOH, with monodeprotonated 2-hy-droxy-3-meth-oxy-benzaldehyde thio-semicarbazone as ligands crystallizes in the space group . The asymmetric unit consists of two mononuclear [Co ] cations, one di-thio-nate anion (SO) as counter-anion and seven solvate mol-ecules (four di-methyl-methanamide and three methanol). Each Co ion has a moderately distorted octa-hedral SNO geometry. In the crystal, the components are linked by numerous N-H⋯O and O-H⋯O contacts.
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