A POM-based one-dimensional (1D) chain compound, {BWO[Cu(2,2'-bipy)][Cu(2,2'-bipy)(HO)]}{BWO[Cu(2,2'-bipy)][Cu(2,2'-bipy)(HO)]}·7HO, has been synthesized and structurally characterized, which represents an unprecedented 1D double chain structure with opposite charges. In contrast to common POMs, this compound exhibits a relatively high electrical conductivity of 1.17 × 10 S cm at 25 °C. In addition, its semiconducting properties have also been investigated by application of photoelectrochemical sensing of HO.
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