In this work, we present the synthesis of an alternative precursor for chemical vapour deposition of parylene AF-4 to the widely used standard, octafluoro[2.2]paracyclophane. The standard precursor suffers from uncertainties in its supply chain and its synthesis is of low yield. A comparison between different reaction parameters and solvents is drawn by means of thermal, laboratory-scale and microwave-assisted reactions and quantitative nuclear magnetic resonance (qNMR) studies.
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| http://www.ncbi.nlm.nih.gov/pmc/articles/PMC8059661 | PMC |
| http://dx.doi.org/10.1098/rsos.201921 | DOI Listing |
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