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NMR spectroscopy derived plasma biomarkers of inflammation in human populations: Influences of age, sex and adiposity.
PLoS One
January 2025
Australian National Phenome Center and Center for Computational and Systems Medicine, Health Futures Institute, Murdoch University, Perth, Western Australia, Australia.
Understanding the distribution and variation in inflammatory markers is crucial for advancing our knowledge of inflammatory processes and evaluating their clinical utility in diagnosing and monitoring acute and chronic disease. 1H NMR spectroscopy of blood plasma and serum was applied to measure a composite panel of inflammatory markers based on acute phase glycoprotein signals (GlycA and GlycB) and sub-regions of the lipoprotein derived Supramolecular Phospholipid Composite signals (SPC1, SPC2 and SPC3) to establish normal ranges in two healthy, predominantly white cohorts from Australia (n = 398) and Spain (n = 80; ages 20-70 years). GlycA, GlycB, SPC1 and SPC3 were not significantly impacted by age or sex, but SPC2 (an HDL-related biomarker) was significantly higher in women across all age ranges by an average of 33.
View Article and Find Full Text PDFSynthesis of a PdL Hydrazone Molecular Cage Through Multiple Reaction Pathways.
Int J Mol Sci
November 2024
Instituto Interuniversitario de Investigación de Reconocimiento Molecular y Desarrollo Tecnológico (IDM), Universitat Politècnica de València, Universitat de València, Camino de Vera s/n, 46022 Valencia, Spain.
Molecular cages are preorganized molecules with a central cavity, typically formed through the reaction of their building blocks through chemical bonds. This requires, in most cases, forming and breaking reversible bonds during the cage formation reaction pathway for error correction to drive the reaction to the cage product. In this work, we focus on both Pd-ligand and hydrazone bonds implemented in the structure of a PdL hydrazone molecular cage.
View Article and Find Full Text PDFCorrection to: Computational study of the supramolecular complexation of azocompounds with cucurbit[7]uril: effects on the production and release of free radicals.
J Mol Model
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Departamento de Química Física, Escuela de Química, Facultad de Química y de Farmacia, Pontificia Universidad Católica de Chile, Av. Vicuña Mackenna 4860, Macul, 7820436, Santiago, Chile.
A tetrathiafulvalene-containing covalent organic nanobelt: preparation, crystal structure and application for sodium-ion batteries.
Chem Sci
December 2024
Department of Materials Science and Engineering, City University of Hong Kong Hong Kong SAR 999077 P. R. China
Developing single crystals of covalent organic polymers (COPs) is highly attractive as they can afford precise structural information for studying internal interactions. Employing dative boron-nitrogen (B-N) bonds to construct single-crystalline COPs is feasible since the dynamic linkages can self-correct errors, thus improving crystallization. In this project, we develop a single-crystal COP with a nanobelt structure, namely CityU-26, B-N-driven-assembly between 4,4',5,5'-tetrakis(4-(pyridin-4-yl)phenyl)-2,2'-bi(1,3-dithiolylidene) and 1,4-bis(benzodioxaborole) benzene.
View Article and Find Full Text PDFRevealing the mechanism of bifunctional PtLa electrocatalyst for highly efficient methanol oxidation, hydrogen evolution, and coupling reaction.
J Colloid Interface Sci
February 2025
College of Chemistry and Chemical Engineering, Xiamen University, Xiamen 361005, China.
The development of clean energy solutions, such as fuel cells and hydrogen energy, is crucial for addressing the global energy shortage. Platinum (Pt)-based catalysts are widely used in fuel cells and hydrogen energy generation (for example, via water electrolysis). However, reducing the amount of Pt used while maintaining the catalytic performance of such catalysts is essential.
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