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The reactions of sodium amidoborane (NaNHBH) with NiBr have been investigated, and the results showed that black precipitate including the NiBNH composites could be obtained. From the aqueous solution of the precipitate , the hydrolysis product Ni-B () was isolated and characterized. Both the in situ formed precipitate and the hydrolysis product can catalyze the formation of Na[BH(NHBH)H]. CoCl showed comparable performance with NiBr. Based on these results, a facile method for the synthesis of Na[BH(NHBH)H] has been developed. This work provides insights into studying experimental methods for the synthesis of long B/N chain complexes and developing boron and nitrogen chemistry.
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| http://dx.doi.org/10.1021/acs.inorgchem.1c00071 | DOI Listing |
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